Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline
The reaction of benzyl o-vanillin 1 with ophenylenediamine 2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-benzyloxy-3- methoxybenzylidene) benzeneamine 2. The intermediate 2 is isolated and obtained as single crystals and their structures were determined...
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| Main Authors: | , , |
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| Format: | Conference or Workshop Item |
| Language: | English |
| Published: |
icic-bme
2009
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| Subjects: | |
| Online Access: | http://irep.iium.edu.my/5353/2/IEEE_Proceedings-Mohammad%5B2extract%5D.pdf http://irep.iium.edu.my/5353/ |
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| Institution: | Universiti Islam Antarabangsa Malaysia |
| Language: | English |
| Summary: | The reaction of benzyl o-vanillin 1 with ophenylenediamine
2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-benzyloxy-3-
methoxybenzylidene) benzeneamine 2. The intermediate 2 is
isolated and obtained as single crystals and their structures were determined and studied by x-ray crystallography. The complete assignments of 2 were made using FTIR, HRMS, 1D and 2D NMR including 13C, COSY, HMQC and HMBC in CDCl3 and will be discussed. |
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