Characterization of Bi2S3 nanorods and nano-structured flowers prepared by a hydrothermal method
Bismuth sulfide nanorods and nano-structured flowers were synthesized by hydrothermal reaction of bismuth nitrate pentahydrate and thiourea solutions, containing 1 and 2 ml of 65% HNO3, respectively. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning...
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| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
| Published: |
2014
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| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-67349278521&partnerID=40&md5=4f45ed2c4fe0d98caca9d074dfb7ed10 http://cmuir.cmu.ac.th/handle/6653943832/5848 |
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| Institution: | Chiang Mai University |
| Language: | English |
| Summary: | Bismuth sulfide nanorods and nano-structured flowers were synthesized by hydrothermal reaction of bismuth nitrate pentahydrate and thiourea solutions, containing 1 and 2 ml of 65% HNO3, respectively. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and high resolution TEM (HRTEM), the products were specified as orthorhombic Bi2S3 in the shapes of nanorods and flower-like clusters of nanorods, with the growth of nanorods in the [001] direction. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment. © 2009 Elsevier B.V. All rights reserved. |
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