Characterization of PbS with different morphologies produced using a cyclic microwave radiation

PbS was produced from different lead (Pb(CH3COO)2·H2O, PbCl2·2.5H2O, Pb(NO3)2) and sulfur (CH3CSNH2, CH5N3S, NH2CSNH2) sources in propylene glycol using a cyclic microwave radiation at different powers and prolonged times. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area elec...

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Main Authors:	Anukorn Phuruangrat, Titipun Thongtem, Somchai Thongtem
Format:	Journal
Published:	2018
Subjects:	Chemistry Materials Science Physics and Astronomy
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=51449109844&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60243
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Institution:	Chiang Mai University

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spelling	th-cmuir.6653943832-602432018-09-10T03:48:16Z Characterization of PbS with different morphologies produced using a cyclic microwave radiation Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Chemistry Materials Science Physics and Astronomy PbS was produced from different lead (Pb(CH3COO)2·H2O, PbCl2·2.5H2O, Pb(NO3)2) and sulfur (CH3CSNH2, CH5N3S, NH2CSNH2) sources in propylene glycol using a cyclic microwave radiation at different powers and prolonged times. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED) techniques. The interpreted and simulated patterns are in good accord. Raman spectrometer revealed the presence of vibrations at 138, 273 and 439 cm-1. Different morphologies (nano-sized particles, hexapods, cubes, ferns and magic squares) were characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM). The product morphologies were influenced by the starting agents, microwave powers and prolonged times. © 2008 Elsevier B.V. All rights reserved. 2018-09-10T03:39:49Z 2018-09-10T03:39:49Z 2008-09-30 Journal 01694332 2-s2.0-51449109844 10.1016/j.apsusc.2008.01.059 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=51449109844&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60243
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Chemistry Materials Science Physics and Astronomy
spellingShingle	Chemistry Materials Science Physics and Astronomy Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Characterization of PbS with different morphologies produced using a cyclic microwave radiation
description	PbS was produced from different lead (Pb(CH3COO)2·H2O, PbCl2·2.5H2O, Pb(NO3)2) and sulfur (CH3CSNH2, CH5N3S, NH2CSNH2) sources in propylene glycol using a cyclic microwave radiation at different powers and prolonged times. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED) techniques. The interpreted and simulated patterns are in good accord. Raman spectrometer revealed the presence of vibrations at 138, 273 and 439 cm-1. Different morphologies (nano-sized particles, hexapods, cubes, ferns and magic squares) were characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM). The product morphologies were influenced by the starting agents, microwave powers and prolonged times. © 2008 Elsevier B.V. All rights reserved.
format	Journal
author	Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem
author_facet	Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem
author_sort	Anukorn Phuruangrat
title	Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_short	Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_full	Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_fullStr	Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_full_unstemmed	Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_sort	characterization of pbs with different morphologies produced using a cyclic microwave radiation
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=51449109844&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60243
_version_	1681425399941169152

Characterization of PbS with different morphologies produced using a cyclic microwave radiation

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