Microwave-assisted synthesis of CePO 4 nanorod phosphor with violet emission

Monoclinic and hexagonal CePO 4 nanoparticles and nanorods were successfully synthesized from Ce(NO 3) 3·6H 2O and Na 3PO 4·12H...

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Main Authors: Ekthammathat N., Thongtem T., Phuruangrat A., Thongtem S.
格式: Article
語言:English
出版: 2014
在線閱讀:http://www.scopus.com/inward/record.url?eid=2-s2.0-84855705021&partnerID=40&md5=21c0af7692dd327e5e7e1309e1415bc7
http://cmuir.cmu.ac.th/handle/6653943832/6408
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spelling th-cmuir.6653943832-64082014-08-30T03:24:10Z Microwave-assisted synthesis of CePO 4 nanorod phosphor with violet emission Ekthammathat N. Thongtem T. Phuruangrat A. Thongtem S. Monoclinic and hexagonal CePO 4 nanoparticles and nanorods were successfully synthesized from Ce(NO 3) 3·6H 2O and Na 3PO 4·12H 2O solutions at pH 1-5 by a 180 W microwave radiation for 60 min. The products were characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, and scanning electron microscopy (SEM). XRD patterns revealed that the products are hexagonal CePO 4 structures at pH 2-5, and monoclinic CePO 4 structures at pH 1. SEM characterization shows that these products were nanoparticles, short nanorods, and long nanorods, controlled by the pH of the precursor solutions. Optical properties of the nanorods were also investigated by ultraviolet-visible (UV-vis) and photoluminescence (PL) spectroscopy. © The Nonferrous Metals Society of China and Springer-Verlag Berlin Heidelberg 2011. 2014-08-30T03:24:10Z 2014-08-30T03:24:10Z 2011 Article 10010521 10.1007/s12598-011-0431-1 RARME http://www.scopus.com/inward/record.url?eid=2-s2.0-84855705021&partnerID=40&md5=21c0af7692dd327e5e7e1309e1415bc7 http://cmuir.cmu.ac.th/handle/6653943832/6408 English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description Monoclinic and hexagonal CePO 4 nanoparticles and nanorods were successfully synthesized from Ce(NO 3) 3·6H 2O and Na 3PO 4·12H 2O solutions at pH 1-5 by a 180 W microwave radiation for 60 min. The products were characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, and scanning electron microscopy (SEM). XRD patterns revealed that the products are hexagonal CePO 4 structures at pH 2-5, and monoclinic CePO 4 structures at pH 1. SEM characterization shows that these products were nanoparticles, short nanorods, and long nanorods, controlled by the pH of the precursor solutions. Optical properties of the nanorods were also investigated by ultraviolet-visible (UV-vis) and photoluminescence (PL) spectroscopy. © The Nonferrous Metals Society of China and Springer-Verlag Berlin Heidelberg 2011.
format Article
author Ekthammathat N.
Thongtem T.
Phuruangrat A.
Thongtem S.
spellingShingle Ekthammathat N.
Thongtem T.
Phuruangrat A.
Thongtem S.
Microwave-assisted synthesis of CePO 4 nanorod phosphor with violet emission
author_facet Ekthammathat N.
Thongtem T.
Phuruangrat A.
Thongtem S.
author_sort Ekthammathat N.
title Microwave-assisted synthesis of CePO 4 nanorod phosphor with violet emission
title_short Microwave-assisted synthesis of CePO 4 nanorod phosphor with violet emission
title_full Microwave-assisted synthesis of CePO 4 nanorod phosphor with violet emission
title_fullStr Microwave-assisted synthesis of CePO 4 nanorod phosphor with violet emission
title_full_unstemmed Microwave-assisted synthesis of CePO 4 nanorod phosphor with violet emission
title_sort microwave-assisted synthesis of cepo 4 nanorod phosphor with violet emission
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-84855705021&partnerID=40&md5=21c0af7692dd327e5e7e1309e1415bc7
http://cmuir.cmu.ac.th/handle/6653943832/6408
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