Characterization of ZnO flowers of hexagonal prisms with planar and hexagonal pyramid tips grown on Zn substrates by a hydrothermal process

Flower-like ZnO crystals on zinc substrates were synthesized by a simple hydrothermal method in different solutions containing 0.05, 0.10, 0.20, 0.30 and 0.40 g LiOH. X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM), transmission electron mi...

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Main Authors: Ekthammathat N., Thongtem T., Phuruangrat A., Thongtem S.
格式: Article
語言:English
出版: 2014
在線閱讀:http://www.scopus.com/inward/record.url?eid=2-s2.0-84870510014&partnerID=40&md5=3b9fb4302e7c4221558aa566604219ce
http://cmuir.cmu.ac.th/handle/6653943832/6991
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總結:Flower-like ZnO crystals on zinc substrates were synthesized by a simple hydrothermal method in different solutions containing 0.05, 0.10, 0.20, 0.30 and 0.40 g LiOH. X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and selected area electron diffraction (SAED) showed that the products were wurtzite hexagonal ZnO flowers, composed of single crystalline hexagonal prisms grown along the [0 0 0 1] direction with planar and hexagonal pyramid tips, including the Zn-O stretching vibration at 411.5 cm-1. Photoluminescence (PL), excited by a 215 nm wavelength at room temperature, exhibited strong green emission at 543 nm. © 2012 Elsevier Ltd. All rights reserved.