Synthesis Of 4-(4-Methoxy -Phenyl)-3-Butene-2-On And The Activity Test As A Fruit Flies A Tract Ant
4-(4-methoxyphenyl)-3-buten-2-on has been synthesized from p-anisaldehyde and acetone via aldol condensation. The reaction was performed at room temperature under basic condition for 12 hours to give brown solid of product (m.p 64-68>C) in 66.19 % yield. p-anisaldehyde itself was produced from ox...
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| Format: | Article NonPeerReviewed |
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[Yogyakarta] : Universitas Gadjah Mada
2008
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| Online Access: | https://repository.ugm.ac.id/27344/ http://i-lib.ugm.ac.id/jurnal/download.php?dataId=10400 |
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| Institution: | Universitas Gadjah Mada |
| Summary: | 4-(4-methoxyphenyl)-3-buten-2-on has been synthesized from p-anisaldehyde and acetone via aldol condensation. The reaction was performed at room temperature under basic condition for 12 hours to give brown solid of product (m.p 64-68>C) in 66.19 % yield. p-anisaldehyde itself was produced from oxidation of anetol major component of anise oil by the use of potassium permanganate as a oxidator. The structure of the products was analyzed by FTIR, 1 H NMR and GC-MS. Activity fest of 4-(4-methoxyphenyQ-3-buten-2-on as an attractant was carried out in Sleman with methyl eugenol as a reference. The result showed that 4-(4-methoxyphenyQ-3-buten-2-on was inactive compound as a fruit flies attractant and some of fruit flies, i.e. Bactrocera papayae, B: carambolae, B. umbrosa and B. abdolonginqua was found on the test area.
Keywords: 4-(4-metoxy-phenyl)~3-butene-2-on, Bactrocera spp., attractant. |
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