THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE

It was conducted a research about the addition effect of sulphanilic acid to the synthesis 3,4- methylenedioxybenzaldehyde from the isosafrole using reagents of sodium dichromate, sulphuric acid, and sulphanilic acid. The separation and purification of product were performed using the chromatograph...

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Main Author: Perpustakaan UGM, i-lib
Format: Article NonPeerReviewed
Published: [Yogyakarta] : Universitas Gadjah Mada 2011
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Online Access:https://repository.ugm.ac.id/29248/
http://i-lib.ugm.ac.id/jurnal/download.php?dataId=12311
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spelling id-ugm-repo.292482014-06-18T00:23:21Z https://repository.ugm.ac.id/29248/ THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE Perpustakaan UGM, i-lib Jurnal i-lib UGM It was conducted a research about the addition effect of sulphanilic acid to the synthesis 3,4- methylenedioxybenzaldehyde from the isosafrole using reagents of sodium dichromate, sulphuric acid, and sulphanilic acid. The separation and purification of product were performed using the chromatographycolumn. The purity of the result was tested using thin layer chromatographyand determination of the melting point. Furthermore, it was identified its structure using infrared spectrophoto meter, 1H and 13C nuclear magnetic resonance spectrometry, and mass spectrometry. The experimental result showed that the percentage yield of 3,4- methylenedioxybenzaldehyde with addition sulphanilic acid was 79.54%. [Yogyakarta] : Universitas Gadjah Mada 2011 Article NonPeerReviewed Perpustakaan UGM, i-lib (2011) THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE. Jurnal i-lib UGM. http://i-lib.ugm.ac.id/jurnal/download.php?dataId=12311
institution Universitas Gadjah Mada
building UGM Library
country Indonesia
collection Repository Civitas UGM
topic Jurnal i-lib UGM
spellingShingle Jurnal i-lib UGM
Perpustakaan UGM, i-lib
THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE
description It was conducted a research about the addition effect of sulphanilic acid to the synthesis 3,4- methylenedioxybenzaldehyde from the isosafrole using reagents of sodium dichromate, sulphuric acid, and sulphanilic acid. The separation and purification of product were performed using the chromatographycolumn. The purity of the result was tested using thin layer chromatographyand determination of the melting point. Furthermore, it was identified its structure using infrared spectrophoto meter, 1H and 13C nuclear magnetic resonance spectrometry, and mass spectrometry. The experimental result showed that the percentage yield of 3,4- methylenedioxybenzaldehyde with addition sulphanilic acid was 79.54%.
format Article
NonPeerReviewed
author Perpustakaan UGM, i-lib
author_facet Perpustakaan UGM, i-lib
author_sort Perpustakaan UGM, i-lib
title THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE
title_short THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE
title_full THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE
title_fullStr THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE
title_full_unstemmed THE ADDITION EFFECT OF SULPHANILIC ACID TO THE SYNTHESIS OF 3,4-METHYLENEDIOXYBENZALDEHYDE
title_sort addition effect of sulphanilic acid to the synthesis of 3,4-methylenedioxybenzaldehyde
publisher [Yogyakarta] : Universitas Gadjah Mada
publishDate 2011
url https://repository.ugm.ac.id/29248/
http://i-lib.ugm.ac.id/jurnal/download.php?dataId=12311
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