Preparation of nanosilica powder using rice husk via precipitation method
Silica in nanoscale has various superior properties which leads to a wide range of applications. Most researches used and metal alkoxides as the sources but very few researches attempted at preparing nanosilica powder from the agricultural waste which environmental friendly and inexpensive. This...
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| Main Authors: | , , , , |
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| Format: | Conference or Workshop Item |
| Language: | English English |
| Published: |
Trans Tech Publications Ltd
2020
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| Subjects: | |
| Online Access: | http://irep.iium.edu.my/83682/1/83682_Preparation%20of%20Nanosilica%20Powder%20Using_latest.pdf http://irep.iium.edu.my/83682/2/83682_Preparation%20of%20Nanosilica%20Powder%20Using_scopus.pdf http://irep.iium.edu.my/83682/ https://www.scientific.net/MSF.1010.501 |
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| Institution: | Universiti Islam Antarabangsa Malaysia |
| Language: | English English |
| Summary: | Silica in nanoscale has various superior properties which leads to a wide range of
applications. Most researches used and metal alkoxides as the sources but very few
researches attempted at preparing nanosilica powder from the agricultural waste
which environmental friendly and inexpensive. This research is presented as the
studies of optimization of parameters involved during preparation, aimed to improve
the purity of silica produced. In this work, rice husk ash (RHA) precursor was subjected
to precipitation method in order to produce nanosilica powder. Acid leaching and
thermal treatment were done as a pre-synthesis process. The process parameters that
have been studied were the reuxed NaOH concentration, heating time, and temperature, in which the
properties were then evaluated during characterization process. The results from X-Ray Flourescence (XRF)
conrmed that it is possible to extract 100% purity of silica from RHA treated by the combination of thermal
treatment, acid leaching, reuxed with 2.5 M of NaOH and heated at 50°C for 48 hours. X-Ray Diraction
(XRD) illustrated that the produced silica is in amorphous state. Meanwhile, the mean particle size of the
spherical shape of silica obtained ranging from 44.7 nm to 1.23 μm. Therefore, the best mean particle size
obtained was by using the sample reuxed with 2.5 M NaOH and heated at 50°C for 48 hours, which were
conrmed by Scanning Electron Microscope (SEM) and Field Emission Scanning Electron Microscope (FESEM).
These ndings on the optimum parameters indicate the successful production of highest purity of nanosilica
powder with nanoscaled particle size. |
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