Subcritical water extraction of low methoxyl pectin from pomelo ( Citrus grandis (L.) Osbeck) peels

Low methoxyl (LM) pectin was extracted from pomelo peels using subcritical water in a dynamic mode. The effects of pressure and temperature were analyzed through a face-centred central composite design. Extraction yield and the rate of extraction were found to be predominantly influenced by temperat...

Full description

Saved in:
Bibliographic Details
Main Authors: Liew, Shan Qin, Teoh, Wen Hui, Tan, Chee Keong, Yusoff, Rozita, Ngoh, Gek Cheng
Format: Article
Published: Elsevier 2018
Subjects:
Online Access:http://eprints.um.edu.my/21462/
https://doi.org/10.1016/j.ijbiomac.2018.05.013
Tags: Add Tag
No Tags, Be the first to tag this record!
Institution: Universiti Malaya
Description
Summary:Low methoxyl (LM) pectin was extracted from pomelo peels using subcritical water in a dynamic mode. The effects of pressure and temperature were analyzed through a face-centred central composite design. Extraction yield and the rate of extraction were found to be predominantly influenced by temperature. Optimization of the subcritical water extraction (SWE) yielded an optimized operating condition of 120 °C and 30 bar with a predicted pectin yield of 18.8%. The corresponding experimental yield was 19.6%, which is in close agreement with the predicted data. The pectin obtained from the optimized condition was further analyzed for its physicochemical properties. The kinetics of the SWE was also evaluated whereby the one-site kinetic desorption model was found to be in good agreement with experimental data (R2 > 0.94).