Synthesis of titanium dioxide nanoparticles via sucrose ester micelle-mediated hydrothermal processing route

Titanium dioxide nanoparticles were synthesized via low-temperature sucrose ester micelle-mediated hydrothermal processing route using titanium isopropoxide as the precursor. X-ray diffractometer revealed that the samples possessed a mixed crystalline phases consisting of anatase and brookite in whi...

Full description

Saved in:
Bibliographic Details
Main Authors: Anwar, N.S., Kassim, A., Lim, H.N., Zakarya, S.A., Huang, N.M.
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2010
Subjects:
Online Access:http://eprints.um.edu.my/5363/1/Synthesis_of_titanium_dioxide_nanoparticles_via_sucrose_ester_micelle-mediated_hydrothermal_processing_route.pdf
http://eprints.um.edu.my/5363/
Tags: Add Tag
No Tags, Be the first to tag this record!
Institution: Universiti Malaya
Language: English
Description
Summary:Titanium dioxide nanoparticles were synthesized via low-temperature sucrose ester micelle-mediated hydrothermal processing route using titanium isopropoxide as the precursor. X-ray diffractometer revealed that the samples possessed a mixed crystalline phases consisting of anatase and brookite in which anatase was the main phase. Upon increasing the hydrothermal reaction temperature, the degree of crystallinity of the nanoparticles improved and their morphology transformed from bundles of needles to rods and to spheres. Photocatalytic behaviour of the as-synthesized nanoparticles was investigated by photodegradation of methylene blue solution in an ultraviolet A irradiating photoreactor. The assynthesized nanoparticles exhibited higher photocatalytic performance as compared to the commercial counterpart.