N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate
The asymmetric unit of the title compound, C(22)H(28)N(2)O(3)·CH(4)O, consists of two independent Schiff base mol-ecules and two independent methanol solvent mol-ecules. In one Schiff base mol-ecule, the 2-hydr-oxy group forms an intra-molecular hydrogen bond with the amide O atom, whereas in the ot...
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2008
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my.um.eprints.9242019-01-31T02:01:55Z http://eprints.um.edu.my/924/ N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate Yehye, W.A. Ariffin, A. Ng, S.W. QD Chemistry The asymmetric unit of the title compound, C(22)H(28)N(2)O(3)·CH(4)O, consists of two independent Schiff base mol-ecules and two independent methanol solvent mol-ecules. In one Schiff base mol-ecule, the 2-hydr-oxy group forms an intra-molecular hydrogen bond with the amide O atom, whereas in the other Schiff base mol-ecule, the 2-hydr-oxy-substituted benzene ring is oriented so that the 2-hydr-oxy group serves as hydrogen-bond acceptor for the amide NH group. In the crystal structure, Schiff base mol-ecules inter-act with methanol solvent to furnish a hydrogen-bonded chain. International Union of Crystallography 2008 Article PeerReviewed Yehye, W.A. and Ariffin, A. and Ng, S.W. (2008) N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate. Acta Crystallographica Section E: Structure Reports Online, 64 (Pt 8). o1452. ISSN 1600-5368 http://www.ncbi.nlm.nih.gov/pubmed/21203167 21203167 |
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QD Chemistry Yehye, W.A. Ariffin, A. Ng, S.W. N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate |
| description |
The asymmetric unit of the title compound, C(22)H(28)N(2)O(3)·CH(4)O, consists of two independent Schiff base mol-ecules and two independent methanol solvent mol-ecules. In one Schiff base mol-ecule, the 2-hydr-oxy group forms an intra-molecular hydrogen bond with the amide O atom, whereas in the other Schiff base mol-ecule, the 2-hydr-oxy-substituted benzene ring is oriented so that the 2-hydr-oxy group serves as hydrogen-bond acceptor for the amide NH group. In the crystal structure, Schiff base mol-ecules inter-act with methanol solvent to furnish a hydrogen-bonded chain. |
| format |
Article |
| author |
Yehye, W.A. Ariffin, A. Ng, S.W. |
| author_facet |
Yehye, W.A. Ariffin, A. Ng, S.W. |
| author_sort |
Yehye, W.A. |
| title |
N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate |
| title_short |
N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate |
| title_full |
N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate |
| title_fullStr |
N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate |
| title_full_unstemmed |
N'-(3,5-Di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate |
| title_sort |
n'-(3,5-di-tert-butyl-4-hydroxy-benzyl-idene)-2-hydroxy-benzohydrazide methanol solvate |
| publisher |
International Union of Crystallography |
| publishDate |
2008 |
| url |
http://eprints.um.edu.my/924/ http://www.ncbi.nlm.nih.gov/pubmed/21203167 |
| _version_ |
1643686653411196928 |