Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide
The crystal and molecular structure of (RS)-N-Tert-butyl-2-anilino-3,3-dirnethylbutanamide, a derivative of an amino acid that was obtained by highly selective cleavage of 1,3-di-tert-butylaziridinone by aniline, is described. The racemic mixture of the amide crystallizes in the space grot)p P 2in w...
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1997
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my.ump.umpir.47722018-01-22T01:39:25Z http://umpir.ump.edu.my/id/eprint/4772/ Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide M. M., Yusoff Reibenspies, Joseph H. Talaty, Erach R. Q Science (General) QD Chemistry The crystal and molecular structure of (RS)-N-Tert-butyl-2-anilino-3,3-dirnethylbutanamide, a derivative of an amino acid that was obtained by highly selective cleavage of 1,3-di-tert-butylaziridinone by aniline, is described. The racemic mixture of the amide crystallizes in the space grot)p P 2in with four molecules per unit cell. Crystal Data: a - 10.483(2) A, h - 6.206(I) A, c = 24.767(5) A, [3 - 90.39(3), V = 1611.5(6) A ~, R(F)[I > 2r = 0.0679, wR(F 2) [1 > 2or(l)] = 0. 1148. Springer 1997-12 Article PeerReviewed M. M., Yusoff and Reibenspies, Joseph H. and Talaty, Erach R. (1997) Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide. Journal of Chemical Crystallography, 27 (12). pp. 727-730. ISSN 1074-1542 (print), 1572-8854 (online) http://dx.doi.org/10.1007/BF02576552 DOI: 10.1007/BF02576552 |
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Q Science (General) QD Chemistry M. M., Yusoff Reibenspies, Joseph H. Talaty, Erach R. Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| description |
The crystal and molecular structure of (RS)-N-Tert-butyl-2-anilino-3,3-dirnethylbutanamide, a derivative of an amino acid that was obtained by highly selective cleavage of 1,3-di-tert-butylaziridinone by aniline, is described. The racemic mixture of the amide crystallizes in the space grot)p P 2in with four molecules per unit cell. Crystal Data: a - 10.483(2) A, h - 6.206(I) A, c = 24.767(5) A, [3 - 90.39(3), V = 1611.5(6) A ~, R(F)[I > 2r = 0.0679, wR(F 2) [1 > 2or(l)] = 0. 1148.
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| format |
Article |
| author |
M. M., Yusoff Reibenspies, Joseph H. Talaty, Erach R. |
| author_facet |
M. M., Yusoff Reibenspies, Joseph H. Talaty, Erach R. |
| author_sort |
M. M., Yusoff |
| title |
Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_short |
Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_full |
Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_fullStr |
Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_full_unstemmed |
Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| title_sort |
synthesis and x-ray analysis of (rs)-n-tert-butyl-2-anilino- 3,3-dimethylbutanamide |
| publisher |
Springer |
| publishDate |
1997 |
| url |
http://umpir.ump.edu.my/id/eprint/4772/ http://dx.doi.org/10.1007/BF02576552 |
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