Effect of process parameters on the production of Ti3SiC2 via modified-SHS through arc melting
International Conference on X-Rays and Related Techniques in Research and Industry (ICXRI 2010) jointly organized by Universiti Malaysia Perlis (UniMAP) and X-Ray Application Malaysia Society (XAPP), 9th - 10th June 2010 at Aseania Resort Langkawi, Malaysia.
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Universiti Malaysia Perlis
2010
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my.unimap-101682010-11-09T04:46:33Z Effect of process parameters on the production of Ti3SiC2 via modified-SHS through arc melting Julie J., Mohamed Yau, C. Siong Zainal A., Ahmad Ti3SiC2 Self-propagating high temperature synthesis (SHS) Arc melting International Conference on X-Rays & Related Techniques in Research & Industry (ICXRI) International Conference on X-Rays and Related Techniques in Research and Industry (ICXRI 2010) jointly organized by Universiti Malaysia Perlis (UniMAP) and X-Ray Application Malaysia Society (XAPP), 9th - 10th June 2010 at Aseania Resort Langkawi, Malaysia. Ti3SiC2 was synthesized by modified-SHS system through arc melting. Elemental powder of titanium, silicon, and graphite were weighed according to the stoichiometric ratio of Ti:Si:C = 3:1:2. The powders were mixed and milled by high speed mill for 1 hour. 120 MPa of pressure is used for the compaction. The samples were sent for arc melting process and the effect of arc melting duration (60s, 75s and 90s) was studied. The welding current was varied (70A, 100A, and 130A) to get the best parameters to produce Ti3SiC2 in high composition. The samples were sent for XRD analysis and SEM observation. For arc melting, the best composition of Ti3SiC2 was produced with 100A welding current for 90s instead of impurity TiC formation. Hence, Ti3SiC2 can be produced via modified-SHS through arc melting with mixing duration of 1 hour using high speed mill, and arc melting duration of 90s with weld current of 100A. 2010-11-09T04:46:33Z 2010-11-09T04:46:33Z 2010-06-09 Working Paper p.315-318 978-967-5760-02-0 http://hdl.handle.net/123456789/10168 en Proceedings of the International Conference on X-Rays & Related Techniques in Research & Industry (ICXRI) 2010 Universiti Malaysia Perlis School of Materials Engineering & School of Environmental Engineering |
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English |
| topic |
Ti3SiC2 Self-propagating high temperature synthesis (SHS) Arc melting International Conference on X-Rays & Related Techniques in Research & Industry (ICXRI) |
| spellingShingle |
Ti3SiC2 Self-propagating high temperature synthesis (SHS) Arc melting International Conference on X-Rays & Related Techniques in Research & Industry (ICXRI) Julie J., Mohamed Yau, C. Siong Zainal A., Ahmad Effect of process parameters on the production of Ti3SiC2 via modified-SHS through arc melting |
| description |
International Conference on X-Rays and Related Techniques in Research and Industry (ICXRI 2010) jointly organized by Universiti Malaysia Perlis (UniMAP) and X-Ray Application Malaysia Society (XAPP), 9th - 10th June 2010 at Aseania Resort Langkawi, Malaysia. |
| format |
Working Paper |
| author |
Julie J., Mohamed Yau, C. Siong Zainal A., Ahmad |
| author_facet |
Julie J., Mohamed Yau, C. Siong Zainal A., Ahmad |
| author_sort |
Julie J., Mohamed |
| title |
Effect of process parameters on the production of Ti3SiC2 via modified-SHS through arc melting |
| title_short |
Effect of process parameters on the production of Ti3SiC2 via modified-SHS through arc melting |
| title_full |
Effect of process parameters on the production of Ti3SiC2 via modified-SHS through arc melting |
| title_fullStr |
Effect of process parameters on the production of Ti3SiC2 via modified-SHS through arc melting |
| title_full_unstemmed |
Effect of process parameters on the production of Ti3SiC2 via modified-SHS through arc melting |
| title_sort |
effect of process parameters on the production of ti3sic2 via modified-shs through arc melting |
| publisher |
Universiti Malaysia Perlis |
| publishDate |
2010 |
| url |
http://dspace.unimap.edu.my/xmlui/handle/123456789/10168 |
| _version_ |
1643789759045173248 |