Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5)
Alcohols; Crystalline materials; Mixing; Morphology; Organometallics; Palm oil; Pressure vessels; Surface active agents; Direct mixing method; Faceted structures; Metal organic framework; Microwave assisted synthesis; Microwave-assisted methods; Non-surfactant Template; Structural characteristics; S...
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2023
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my.uniten.dspace-227712023-05-29T14:12:09Z Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5) Othman S.Z. Misran H. Affendy W.A. Mahadi N.F. 55548997100 6506899840 57189241496 57189241140 Alcohols; Crystalline materials; Mixing; Morphology; Organometallics; Palm oil; Pressure vessels; Surface active agents; Direct mixing method; Faceted structures; Metal organic framework; Microwave assisted synthesis; Microwave-assisted methods; Non-surfactant Template; Structural characteristics; Synthesis method; Java programming language; alcohol; numerical method; surfactant; temperature gradient; vegetable oil In this work, metal-organic framework (MOF-5) syntheses were successfully synthesized with three different methods namely i) modified direct-mixing method ii) microwave assisted method and iii) autoclave assisted method without using surfactants. Palm oil derived fatty alcohol (PODFA), dodecyl alcohol (C8) was used as renewable non-surfactant template. Four prominent peaks were observed in all three samples attributable to the reflection planes of (200), (220), (400) and (420) of a cubic structure at ca. 2? = 6.9�, 9.6�, 13.7� and 15.2�. The morphology of MOF-5 produced using modified direct-mixing method was faceted structure with average size of ca. 1 ?m. In addition, the morphology of MOF-5 produced using microwave assisted synthesis was cubic structure with average size of ca. 8.34 ?m. However, the morphology of MOF-5 using autoclave assisted method was interpenetrated cubic with average size of ca. 22.65 ?m. Final 2023-05-29T06:12:09Z 2023-05-29T06:12:09Z 2016 Conference Paper 10.1088/1755-1315/32/1/012060 2-s2.0-84966586699 https://www.scopus.com/inward/record.uri?eid=2-s2.0-84966586699&doi=10.1088%2f1755-1315%2f32%2f1%2f012060&partnerID=40&md5=3bac02d70b187914e1802bb1fb647a14 https://irepository.uniten.edu.my/handle/123456789/22771 32 1 12060 All Open Access, Bronze Institute of Physics Publishing Scopus |
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| description |
Alcohols; Crystalline materials; Mixing; Morphology; Organometallics; Palm oil; Pressure vessels; Surface active agents; Direct mixing method; Faceted structures; Metal organic framework; Microwave assisted synthesis; Microwave-assisted methods; Non-surfactant Template; Structural characteristics; Synthesis method; Java programming language; alcohol; numerical method; surfactant; temperature gradient; vegetable oil |
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55548997100 |
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55548997100 Othman S.Z. Misran H. Affendy W.A. Mahadi N.F. |
| format |
Conference Paper |
| author |
Othman S.Z. Misran H. Affendy W.A. Mahadi N.F. |
| spellingShingle |
Othman S.Z. Misran H. Affendy W.A. Mahadi N.F. Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5) |
| author_sort |
Othman S.Z. |
| title |
Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5) |
| title_short |
Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5) |
| title_full |
Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5) |
| title_fullStr |
Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5) |
| title_full_unstemmed |
Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5) |
| title_sort |
effect of synthesis methods using renewable podfa on structural characteristics of metal-organic framework (mof-5) |
| publisher |
Institute of Physics Publishing |
| publishDate |
2023 |
| _version_ |
1806426686429855744 |