Preparation of oil palm EFB derived solid acid catalyst for esterification reaction: Effect of calcination temperature
Biodiesel; Calcination; Catalyst activity; Esterification; Esters; Fruits; Iron compounds; Morphology; Oleic acid; Sulfur compounds; Surface chemistry; Transition metals; Biodiesel production; Calcination temperature; Esterification of oleic acids; Esterification reactions; Oil palm empty fruit bunc...
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Trans Tech Publications Ltd
2023
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my.uniten.dspace-229542023-05-29T14:13:40Z Preparation of oil palm EFB derived solid acid catalyst for esterification reaction: Effect of calcination temperature Krishnan S.G. Pua F.L. Palanisamy K. Nabihah S. 57190370972 36024192100 56803626200 25722192000 Biodiesel; Calcination; Catalyst activity; Esterification; Esters; Fruits; Iron compounds; Morphology; Oleic acid; Sulfur compounds; Surface chemistry; Transition metals; Biodiesel production; Calcination temperature; Esterification of oleic acids; Esterification reactions; Oil palm empty fruit bunch; Oil palm empty fruit bunches (EFB); Solid acid catalysts; Transition metal sulfides; Palm oil Oil palm empty fruit bunch (EFB) is one of the palm biomass produced in abundance after oil extraction in Malaysia. This study was focused to utilize this waste biomass as a beneficial raw materials. EFB was used to prepare new solid acid catalyst for biodiesel production. EFB was converted into solid catalyst via direct impregnation method and it was used to catalyse esterification of oleic acid. Transition metal sulfide salt, Fe2(SO4)3 was impregnated on EFB fibres. Effect of different calcination temperature was studied on the properties of catalyst. The result shows that Fe2(SO4)3 based solid acid catalyst which calcined at 500oC exhibited the highest catalytic activity with 93.90% esterification rate was achieved. The morphology and surface chemistry and function group determination for the solid acid catalyst were characterized by SEM-EDX and FTIR. � 2016 Trans Tech Publications, Switzerland. Final 2023-05-29T06:13:39Z 2023-05-29T06:13:39Z 2016 Conference Paper 10.4028/www.scientific.net/KEM.701.117 2-s2.0-84979643057 https://www.scopus.com/inward/record.uri?eid=2-s2.0-84979643057&doi=10.4028%2fwww.scientific.net%2fKEM.701.117&partnerID=40&md5=561f89f7072e63eb45da80f2f857ed85 https://irepository.uniten.edu.my/handle/123456789/22954 701 117 121 Trans Tech Publications Ltd Scopus |
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| description |
Biodiesel; Calcination; Catalyst activity; Esterification; Esters; Fruits; Iron compounds; Morphology; Oleic acid; Sulfur compounds; Surface chemistry; Transition metals; Biodiesel production; Calcination temperature; Esterification of oleic acids; Esterification reactions; Oil palm empty fruit bunch; Oil palm empty fruit bunches (EFB); Solid acid catalysts; Transition metal sulfides; Palm oil |
| author2 |
57190370972 |
| author_facet |
57190370972 Krishnan S.G. Pua F.L. Palanisamy K. Nabihah S. |
| format |
Conference Paper |
| author |
Krishnan S.G. Pua F.L. Palanisamy K. Nabihah S. |
| spellingShingle |
Krishnan S.G. Pua F.L. Palanisamy K. Nabihah S. Preparation of oil palm EFB derived solid acid catalyst for esterification reaction: Effect of calcination temperature |
| author_sort |
Krishnan S.G. |
| title |
Preparation of oil palm EFB derived solid acid catalyst for esterification reaction: Effect of calcination temperature |
| title_short |
Preparation of oil palm EFB derived solid acid catalyst for esterification reaction: Effect of calcination temperature |
| title_full |
Preparation of oil palm EFB derived solid acid catalyst for esterification reaction: Effect of calcination temperature |
| title_fullStr |
Preparation of oil palm EFB derived solid acid catalyst for esterification reaction: Effect of calcination temperature |
| title_full_unstemmed |
Preparation of oil palm EFB derived solid acid catalyst for esterification reaction: Effect of calcination temperature |
| title_sort |
preparation of oil palm efb derived solid acid catalyst for esterification reaction: effect of calcination temperature |
| publisher |
Trans Tech Publications Ltd |
| publishDate |
2023 |
| _version_ |
1806426630712721408 |