The colloidal stability of water-in-oil-in-water double emulsion stabilized by Pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract

Double emulsion (DE) has recently attracted attention due to its ability to encapsulate hydrophilic and hydrophobic substances and controlled release properties. However, food-grade DE is prone to destabilization due to its complex structure, which makes practical application in the industries diffi...

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Main Authors: Elaine, Elaine, Tan, Chin Ping, Akanda, Md Jahurul Haque, Nyam, Kar Lin
Format: Article
Published: Springer 2024
Online Access:http://psasir.upm.edu.my/id/eprint/113658/
https://link.springer.com/article/10.1007/s11694-024-02684-7?error=cookies_not_supported&code=3b69ac58-812b-4add-8739-9cc3d8ada17d
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Institution: Universiti Putra Malaysia
id my.upm.eprints.113658
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spelling my.upm.eprints.1136582025-02-05T04:18:36Z http://psasir.upm.edu.my/id/eprint/113658/ The colloidal stability of water-in-oil-in-water double emulsion stabilized by Pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract Elaine, Elaine Tan, Chin Ping Akanda, Md Jahurul Haque Nyam, Kar Lin Double emulsion (DE) has recently attracted attention due to its ability to encapsulate hydrophilic and hydrophobic substances and controlled release properties. However, food-grade DE is prone to destabilization due to its complex structure, which makes practical application in the industries difficult. This study investigates the stabilization of DE containing ethanolic kenaf leaf extract using different concentrations of Pickering emulsifier mixture (PEM). PEM consists of sodium caseinate, tween-20, and beta-cyclodextrin at the fixed ratio of 57.9:27.6:14.5% (w/w/w). Key parameters such as droplet size, polydispersity index, creaming index, encapsulation efficiency, and droplet morphology were monitored during 5-week storage at 25 °C. All DE samples remained phase-stable and exhibited increasing viscosity throughout the storage. The droplets displayed a spherical shape, and functional group assessment indicated changes in the molecular interactions after ultrasonic emulsification. DE stabilized by 2.5% and 4.0% (w/w) PEM consistently maintained droplet size and distribution, achieving encapsulation efficiency exceeding 98%. Specifically, DE with 4.0% (w/w) PEM exhibited excellent resistance to pH changes. In conclusion, PEM-stabilized DE remained stable for up to 5 weeks at 25 °C, which facilitates the beneficial uses of double emulsion in food, cosmetic, and medical applications. Springer 2024-07-10 Article PeerReviewed Elaine, Elaine and Tan, Chin Ping and Akanda, Md Jahurul Haque and Nyam, Kar Lin (2024) The colloidal stability of water-in-oil-in-water double emulsion stabilized by Pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract. Journal of Food Measurement and Characterization, 18 (8). pp. 6711-6720. ISSN 2193-4126; eISSN: 2193-4134 https://link.springer.com/article/10.1007/s11694-024-02684-7?error=cookies_not_supported&code=3b69ac58-812b-4add-8739-9cc3d8ada17d 10.1007/s11694-024-02684-7
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
description Double emulsion (DE) has recently attracted attention due to its ability to encapsulate hydrophilic and hydrophobic substances and controlled release properties. However, food-grade DE is prone to destabilization due to its complex structure, which makes practical application in the industries difficult. This study investigates the stabilization of DE containing ethanolic kenaf leaf extract using different concentrations of Pickering emulsifier mixture (PEM). PEM consists of sodium caseinate, tween-20, and beta-cyclodextrin at the fixed ratio of 57.9:27.6:14.5% (w/w/w). Key parameters such as droplet size, polydispersity index, creaming index, encapsulation efficiency, and droplet morphology were monitored during 5-week storage at 25 °C. All DE samples remained phase-stable and exhibited increasing viscosity throughout the storage. The droplets displayed a spherical shape, and functional group assessment indicated changes in the molecular interactions after ultrasonic emulsification. DE stabilized by 2.5% and 4.0% (w/w) PEM consistently maintained droplet size and distribution, achieving encapsulation efficiency exceeding 98%. Specifically, DE with 4.0% (w/w) PEM exhibited excellent resistance to pH changes. In conclusion, PEM-stabilized DE remained stable for up to 5 weeks at 25 °C, which facilitates the beneficial uses of double emulsion in food, cosmetic, and medical applications.
format Article
author Elaine, Elaine
Tan, Chin Ping
Akanda, Md Jahurul Haque
Nyam, Kar Lin
spellingShingle Elaine, Elaine
Tan, Chin Ping
Akanda, Md Jahurul Haque
Nyam, Kar Lin
The colloidal stability of water-in-oil-in-water double emulsion stabilized by Pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract
author_facet Elaine, Elaine
Tan, Chin Ping
Akanda, Md Jahurul Haque
Nyam, Kar Lin
author_sort Elaine, Elaine
title The colloidal stability of water-in-oil-in-water double emulsion stabilized by Pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract
title_short The colloidal stability of water-in-oil-in-water double emulsion stabilized by Pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract
title_full The colloidal stability of water-in-oil-in-water double emulsion stabilized by Pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract
title_fullStr The colloidal stability of water-in-oil-in-water double emulsion stabilized by Pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract
title_full_unstemmed The colloidal stability of water-in-oil-in-water double emulsion stabilized by Pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract
title_sort colloidal stability of water-in-oil-in-water double emulsion stabilized by pickering emulsifier mixture in encapsulating ethanolic kenaf leaves extract
publisher Springer
publishDate 2024
url http://psasir.upm.edu.my/id/eprint/113658/
https://link.springer.com/article/10.1007/s11694-024-02684-7?error=cookies_not_supported&code=3b69ac58-812b-4add-8739-9cc3d8ada17d
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