Difatty acyl urea from corn oil: synthesis and characterization
In this study, difatty acyl urea has been successfully synthesized from corn oil using sodium ethoxide as a catalyst. Ethyl fatty ester and glycerol were produced as by-products. In this reaction, corn oil was refluxed with urea in ethanol. The highest conversion percentage (78%) was obtained when t...
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Main Authors: | , , , |
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Format: | Article |
Language: | English |
Published: |
Japan Oil Chemists' Society
2010
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Online Access: | http://psasir.upm.edu.my/id/eprint/14061/1/Difatty%20acyl%20urea%20from%20corn%20oil.pdf http://psasir.upm.edu.my/id/eprint/14061/ https://www.jstage.jst.go.jp/article/jos/59/3/59_3_157/_article |
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Institution: | Universiti Putra Malaysia |
Language: | English |
Summary: | In this study, difatty acyl urea has been successfully synthesized from corn oil using sodium ethoxide as a catalyst. Ethyl fatty ester and glycerol were produced as by-products. In this reaction, corn oil was refluxed with urea in ethanol. The highest conversion percentage (78%) was obtained when the process was carried out for 8 hours using urea to corn oil ratio of 5.6: 1.0 at 78 degrees C. Both difatty acyl urea and ethyl fatty ester have been characterized using elemental analysis, Fourier transform infrared (FTIR) spectroscopy and (1)H nuclear magnetic resonance (NMR) technique. |
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