Synthesis and characterization of N,N′-carbonyl difatty amides from palm oil
N,N′-Carbonyl difatty amides (CDFAs) have been synthesized from palm oil using sodium ethoxide as catalyst. Ethyl fatty esters (EFEs) were produced as a by-product as well as glycerol. The synthesis was carried out by reflux palm oil and urea in presence of ethanol. In this process, palm oil gave 79...
Saved in:
| Main Authors: | , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Japan Oil Chemists' Society
2009
|
| Online Access: | http://psasir.upm.edu.my/id/eprint/16930/1/Synthesis%20and%20characterization%20of%20N.pdf http://psasir.upm.edu.my/id/eprint/16930/ https://www.jstage.jst.go.jp/article/jos/58/9/58_9_467/_article |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| Institution: | Universiti Putra Malaysia |
| Language: | English |
| id |
my.upm.eprints.16930 |
|---|---|
| record_format |
eprints |
| spelling |
my.upm.eprints.169302015-11-27T07:21:13Z http://psasir.upm.edu.my/id/eprint/16930/ Synthesis and characterization of N,N′-carbonyl difatty amides from palm oil Al-Mulla, Emad A. Jaffar Wan Yunus, Wan Md. Zin Ibrahim, Nor Azowa Ab. Rahman, Mohamad Zaki N,N′-Carbonyl difatty amides (CDFAs) have been synthesized from palm oil using sodium ethoxide as catalyst. Ethyl fatty esters (EFEs) were produced as a by-product as well as glycerol. The synthesis was carried out by reflux palm oil and urea in presence of ethanol. In this process, palm oil gave 79% pure CDFAs after 8 hours and molar ratio of urea to palm oil was 6.2: 1 at 78°C. Both CDFAs and EFEs have been characterized using elemental analysis, Fourier transform infrared (FTIR) spectroscopy and 1H nuclear magnetic resonance (NMR) technique. Japan Oil Chemists' Society 2009 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/16930/1/Synthesis%20and%20characterization%20of%20N.pdf Al-Mulla, Emad A. Jaffar and Wan Yunus, Wan Md. Zin and Ibrahim, Nor Azowa and Ab. Rahman, Mohamad Zaki (2009) Synthesis and characterization of N,N′-carbonyl difatty amides from palm oil. Journal of Oleo Science, 58 (9). pp. 467-471. ISSN 1345-8957; ESSN: 1347-3352 https://www.jstage.jst.go.jp/article/jos/58/9/58_9_467/_article 10.5650/jos.58.467 |
| institution |
Universiti Putra Malaysia |
| building |
UPM Library |
| collection |
Institutional Repository |
| continent |
Asia |
| country |
Malaysia |
| content_provider |
Universiti Putra Malaysia |
| content_source |
UPM Institutional Repository |
| url_provider |
http://psasir.upm.edu.my/ |
| language |
English |
| description |
N,N′-Carbonyl difatty amides (CDFAs) have been synthesized from palm oil using sodium ethoxide as catalyst. Ethyl fatty esters (EFEs) were produced as a by-product as well as glycerol. The synthesis was carried out by reflux palm oil and urea in presence of ethanol. In this process, palm oil gave 79% pure CDFAs after 8 hours and molar ratio of urea to palm oil was 6.2: 1 at 78°C. Both CDFAs and EFEs have been characterized using elemental analysis, Fourier transform infrared (FTIR) spectroscopy and 1H nuclear magnetic resonance (NMR) technique. |
| format |
Article |
| author |
Al-Mulla, Emad A. Jaffar Wan Yunus, Wan Md. Zin Ibrahim, Nor Azowa Ab. Rahman, Mohamad Zaki |
| spellingShingle |
Al-Mulla, Emad A. Jaffar Wan Yunus, Wan Md. Zin Ibrahim, Nor Azowa Ab. Rahman, Mohamad Zaki Synthesis and characterization of N,N′-carbonyl difatty amides from palm oil |
| author_facet |
Al-Mulla, Emad A. Jaffar Wan Yunus, Wan Md. Zin Ibrahim, Nor Azowa Ab. Rahman, Mohamad Zaki |
| author_sort |
Al-Mulla, Emad A. Jaffar |
| title |
Synthesis and characterization of N,N′-carbonyl difatty amides from palm oil |
| title_short |
Synthesis and characterization of N,N′-carbonyl difatty amides from palm oil |
| title_full |
Synthesis and characterization of N,N′-carbonyl difatty amides from palm oil |
| title_fullStr |
Synthesis and characterization of N,N′-carbonyl difatty amides from palm oil |
| title_full_unstemmed |
Synthesis and characterization of N,N′-carbonyl difatty amides from palm oil |
| title_sort |
synthesis and characterization of n,n′-carbonyl difatty amides from palm oil |
| publisher |
Japan Oil Chemists' Society |
| publishDate |
2009 |
| url |
http://psasir.upm.edu.my/id/eprint/16930/1/Synthesis%20and%20characterization%20of%20N.pdf http://psasir.upm.edu.my/id/eprint/16930/ https://www.jstage.jst.go.jp/article/jos/58/9/58_9_467/_article |
| _version_ |
1643826361904660480 |