Effect of heat treatment on thermal diffusivity of Zn/Al layered double hydroxide synthesized using photoflash technique

• Main Authors: Ghaziean, Maryam Ranjbar, Shameli, Kamyar, Mat Yunus, Mahmood, Hussein, Mohd Zobir, Shameli, Kaveh
• Format: Article
• Language: English
• Published: National Institute of Research and Development for Optoelectronics 2014
• Online Access: http://psasir.upm.edu.my/id/eprint/17325/1/Effect%20of%20heat%20treatment%20on%20thermal%20diffusivity%20of%20ZnAl%20layered%20double%20hydroxide%20synthesized%20using%20photoflash%20technique.pdf; http://psasir.upm.edu.my/id/eprint/17325/; http://oam-rc.inoe.ro/index.php?option=magazine&op=view&idu=2316&catid=84
• Institution: Universiti Putra Malaysia

Thermal diffusivity of zinc-aluminum layered double hydroxides was synthesized at different molar ratio of zinc and aluminum salts in the pH=7 and measured by using polyvinlidene diflouride (PVDF) by photoflash technique. The samples were prepared using Zn(NO3)2 and Al(NO3)3 solutions by drop wise addition of NaOH solution with vigorous stirring under nitrogen atmosphere. The samples then heat treated by control an electrical furnace from 200 to 600 °C for 5 hours. Thermal diffusivity was increased for all samples after sintering. The samples were studied by powder x-ray diffraction method, Fourier transform infrared (FTIR), scanning electron microscope (SEM) and thermal diffusivity. Our results indicate the very different role of sintering in the structure and thermal diffusivity of samples.