1D and 2D NMR studies of 2–(2–(BENZYLOXY)–3–METHOXYPHENYL)–1H–BENZIMIDAZOLEF
The reaction of Benzyl o–vanillin 1 and o–phenylene diamine 2 in dichloromethane produced new benzimidazole, 3. The complete assignments of 3 were made using 1D and 2D NMR including COSY, HMQC and HMBC NMR in CDCl3 and acetone–d6. The coupling constants J are reported in Hertz, and the differences i...
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Main Authors: | , , |
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Format: | Article |
Language: | English |
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Universitas Gadjah Mada
2007
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Online Access: | http://eprints.usm.my/37937/1/1D_AND_2D_NMR_STUDIES_OF_2%E2%80%93%282%E2%80%93%28BENZYLOXY%29%E2%80%933%E2%80%93METHOXYPHENYL%29%E2%80%931H%E2%80%93BENZIMIDAZOLE.pdf http://eprints.usm.my/37937/ http://dx.doi.org/10.22146/ijc.422 |
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Institution: | Universiti Sains Malaysia |
Language: | English |
Summary: | The reaction of Benzyl o–vanillin 1 and o–phenylene diamine 2 in dichloromethane produced new benzimidazole, 3. The complete assignments of 3 were made using 1D and 2D NMR including COSY, HMQC and HMBC NMR in CDCl3 and acetone–d6. The coupling constants J are reported in Hertz, and the differences in the peak splittings using both solvents are discussed |
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