Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method

Bi4Ti3O12was synthesized by fuel-free combustion method using Bi(NO3)3.5H2O and Ti[OCH (CH3)2]4 and subsequent calcination. The effect of processing parameters such as Bi addition and Ti addition on the phase formation of Bi4Ti3O12was investigated. X-Ray Diffraction analysis was used to determine...

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主要作者: Al-Amani, Umar
格式: Conference or Workshop Item
語言:English
出版: 2009
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在線閱讀:http://eprints.utem.edu.my/id/eprint/9785/1/RRAMM_and_ASMP_2009.pdf
http://eprints.utem.edu.my/id/eprint/9785/
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機構: Universiti Teknikal Malaysia Melaka
語言: English
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總結:Bi4Ti3O12was synthesized by fuel-free combustion method using Bi(NO3)3.5H2O and Ti[OCH (CH3)2]4 and subsequent calcination. The effect of processing parameters such as Bi addition and Ti addition on the phase formation of Bi4Ti3O12was investigated. X-Ray Diffraction analysis was used to determine the formation of Bi4Ti3O12. Pure Bi4Ti3O12 powder was successfully formed with Ti addition after calcination at 800oC for 3 h. The average crystallite sizes produced were 77.9 nm, 63.6 nm and 51.8 nm with mol ratio of 4:3.1, 4:3.4 and 4:3.6, respectively. The results obtained infer that the relative amount of Ti was identified as limiting reagent in the combustion reaction and was also considered as key factor to achieve single-phase Bi4Ti3O12