The existence of giant magnetocaloric effect and laminar structure in Fe73.5 xCrxSi13.5B9Nb3Cu1

• Main Author: Phung, ThanhPQ
• Format: Article
• Language: English
• Published: Elsevier 2016
• Subjects: Soft magnetic amorphous system
• Online Access: http://repository.vnu.edu.vn/handle/VNU_123/10147
• Institution: Vietnam National University, Hanoi

Amorphous soft magnetic ribbons Fe73.5 xCrxSi13.5B9Nb3Cu1 (x¼1–5) have been fabricated by rapid quenching on a single copper wheel. The differential scanning calorimetry (DSC) patterns showed that the crystallization temperature ofa-Fe(Si) phase is ranging from 542 to 5691C, a little higher than that of pure Finemet (x¼0). With the same annealing regime, the crystallization volume fraction as well as the particle size ofa-Fe(Si) crystallites decreased with increasing Cr amount substituted for Fe in studied samples. Especially, the interesting fact is that the laminar structure of heat-treated ribbons on the surface contacted to copper wheel in the fabricating process has been firstly discovered and explained to be related to the existence of Cr in studied samples. The hysteresis loop measurement indicated that there is the pinning of displacement of domain walls. The giant magnetocaloric effect (GMCE) has been found in amorphous state of the samples. After annealing, the soft magnetic properties of investigated nanocomposite materials are desirably improved.