Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti₃₄Nb via laser powder bed fusion

A parametric experimental study on the role played by the power (P), velocity (VL) and profile (top-hat or Gaussian) of the laser on the porosity, inclusion content and microstructural evolution of in-situ alloyed laser powder bed fusion (LPBF) manufactured Ti34Nb was conducted. For this, alloys wer...

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Main Authors: Huang, Sheng, Narayan, R. Lakshmi, Tan, Joel Heang Kuan, Sing, Swee Leong, Yeong, Wai Yee
Other Authors: School of Mechanical and Aerospace Engineering
Format: Article
Language:English
Published: 2021
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Online Access:https://hdl.handle.net/10356/154109
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spelling sg-ntu-dr.10356-1541092021-12-18T20:12:06Z Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti₃₄Nb via laser powder bed fusion Huang, Sheng Narayan, R. Lakshmi Tan, Joel Heang Kuan Sing, Swee Leong Yeong, Wai Yee School of Mechanical and Aerospace Engineering Singapore Centre for 3D Printing Engineering::Mechanical engineering Additive Manufacturing Powder Bed Fusion A parametric experimental study on the role played by the power (P), velocity (VL) and profile (top-hat or Gaussian) of the laser on the porosity, inclusion content and microstructural evolution of in-situ alloyed laser powder bed fusion (LPBF) manufactured Ti34Nb was conducted. For this, alloys were printed with three sets of processing parameters, in which the above-mentioned parameters were varied but the energy density was held constant. A detailed tomographic and microstructural investigation of these alloys was followed by tensile tests. Observations of melt pools in the single tracks and single stripes were complemented by thermal finite element method (FEM) simulations that studied their evolution. Results show that a top-hat laser profile combined with high P (> 650 W), high VL (> 650 mm/s) and short stripe width scanning strategy forms a large single stripe melt pool that moves slowly and has a low aspect ratio. The large and slow melt pool allows Nb to melt efficiently and minimizes its unmelted content while the low melt pool aspect ratio prevents keyholing that can otherwise result in porosity. These melt pool attributes also favor the formation of a columnar β-Ti microstructure with a strong {100} texture, which has the ideal combination of strength and elastic modulus. The mechanisms of microstructural evolution were explained and the scope of this parameter optimization principle was discussed in the context of further improving the properties of this alloy. National Research Foundation (NRF) Accepted version This research is supported by the National Research Foundation, Prime Minister’s Office, Singapore under its Medium-Sized Centre funding scheme. S. Huang would like to acknowledge Nanyang President’s Graduate Scholarship from Nanyang Technological University for funding the Ph.D. studies. 2021-12-15T06:18:44Z 2021-12-15T06:18:44Z 2021 Journal Article Huang, S., Narayan, R. L., Tan, J. H. K., Sing, S. L. & Yeong, W. Y. (2021). Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti₃₄Nb via laser powder bed fusion. Acta Materialia, 204, 116522-. https://dx.doi.org/10.1016/j.actamat.2020.116522 1359-6454 https://hdl.handle.net/10356/154109 10.1016/j.actamat.2020.116522 2-s2.0-85097578700 204 116522 en Acta Materialia © 2020 Acta Materialia Inc. All rights reserved. This paper was published by Elsevier Ltd. in Acta Materialia and is made available with permission of Acta Materialia Inc. application/pdf
institution Nanyang Technological University
building NTU Library
continent Asia
country Singapore
Singapore
content_provider NTU Library
collection DR-NTU
language English
topic Engineering::Mechanical engineering
Additive Manufacturing
Powder Bed Fusion
spellingShingle Engineering::Mechanical engineering
Additive Manufacturing
Powder Bed Fusion
Huang, Sheng
Narayan, R. Lakshmi
Tan, Joel Heang Kuan
Sing, Swee Leong
Yeong, Wai Yee
Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti₃₄Nb via laser powder bed fusion
description A parametric experimental study on the role played by the power (P), velocity (VL) and profile (top-hat or Gaussian) of the laser on the porosity, inclusion content and microstructural evolution of in-situ alloyed laser powder bed fusion (LPBF) manufactured Ti34Nb was conducted. For this, alloys were printed with three sets of processing parameters, in which the above-mentioned parameters were varied but the energy density was held constant. A detailed tomographic and microstructural investigation of these alloys was followed by tensile tests. Observations of melt pools in the single tracks and single stripes were complemented by thermal finite element method (FEM) simulations that studied their evolution. Results show that a top-hat laser profile combined with high P (> 650 W), high VL (> 650 mm/s) and short stripe width scanning strategy forms a large single stripe melt pool that moves slowly and has a low aspect ratio. The large and slow melt pool allows Nb to melt efficiently and minimizes its unmelted content while the low melt pool aspect ratio prevents keyholing that can otherwise result in porosity. These melt pool attributes also favor the formation of a columnar β-Ti microstructure with a strong {100} texture, which has the ideal combination of strength and elastic modulus. The mechanisms of microstructural evolution were explained and the scope of this parameter optimization principle was discussed in the context of further improving the properties of this alloy.
author2 School of Mechanical and Aerospace Engineering
author_facet School of Mechanical and Aerospace Engineering
Huang, Sheng
Narayan, R. Lakshmi
Tan, Joel Heang Kuan
Sing, Swee Leong
Yeong, Wai Yee
format Article
author Huang, Sheng
Narayan, R. Lakshmi
Tan, Joel Heang Kuan
Sing, Swee Leong
Yeong, Wai Yee
author_sort Huang, Sheng
title Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti₃₄Nb via laser powder bed fusion
title_short Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti₃₄Nb via laser powder bed fusion
title_full Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti₃₄Nb via laser powder bed fusion
title_fullStr Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti₃₄Nb via laser powder bed fusion
title_full_unstemmed Resolving the porosity-unmelted inclusion dilemma during in-situ alloying of Ti₃₄Nb via laser powder bed fusion
title_sort resolving the porosity-unmelted inclusion dilemma during in-situ alloying of ti₃₄nb via laser powder bed fusion
publishDate 2021
url https://hdl.handle.net/10356/154109
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