Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation

In this study, the recrystallization process of selective laser melted (SLM) commercially pure titanium (CP-Ti) was followed by a quasi-in-situ electron backscatter diffraction (EBSD) method at 800 °C and 700 °C. Abnormal grain growth (AGG) initially emerges at the beginning of annealing at 800 °C a...

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Main Authors: Chen, Kewei, Huang, De Jun, Li, Hua, Jia, Ning, Chong, Warren
Other Authors: School of Mechanical and Aerospace Engineering
Format: Article
Language:English
Published: 2022
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Online Access:https://hdl.handle.net/10356/162543
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Institution: Nanyang Technological University
Language: English
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spelling sg-ntu-dr.10356-1625432022-10-28T07:35:35Z Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation Chen, Kewei Huang, De Jun Li, Hua Jia, Ning Chong, Warren School of Mechanical and Aerospace Engineering School of Materials Science and Engineering Singapore Centre for 3D Printing Engineering::Mechanical engineering Engineering::Materials Grain Refining Electron Backscattering Diffraction In this study, the recrystallization process of selective laser melted (SLM) commercially pure titanium (CP-Ti) was followed by a quasi-in-situ electron backscatter diffraction (EBSD) method at 800 °C and 700 °C. Abnormal grain growth (AGG) initially emerges at the beginning of annealing at 800 °C and is primarily caused by strain-induced boundary migration (SIBM). However, at the beginning of annealing at 700 °C, many small equiaxed grains are formed due to more recrystallization nucleation, followed by the formation of AGG resulting from the secondary recrystallization. Based on these findings, appropriate control of the annealing time at 700 °C can mitigate AGG to obtain fine equiaxed grains with weak texture to enhance the tensile properties of SLM CP-Ti. Economic Development Board (EDB) Nanyang Technological University This work is funded by the Economic Development Board Singapore, Nanyang Technological University, and Emerson Asia Pacific Pte Ltd. The authors acknowledge the use of electron microscopy and XRD equipment within the Facilities for Analysis, Characterization, Testing and Simulations (FACTS) at Nanyang Technological University 2022-10-28T07:35:35Z 2022-10-28T07:35:35Z 2022 Journal Article Chen, K., Huang, D. J., Li, H., Jia, N. & Chong, W. (2022). Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation. Scripta Materialia, 209, 114377-. https://dx.doi.org/10.1016/j.scriptamat.2021.114377 1359-6462 https://hdl.handle.net/10356/162543 10.1016/j.scriptamat.2021.114377 2-s2.0-85118542135 209 114377 en Scripta Materialia © 2021 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
institution Nanyang Technological University
building NTU Library
continent Asia
country Singapore
Singapore
content_provider NTU Library
collection DR-NTU
language English
topic Engineering::Mechanical engineering
Engineering::Materials
Grain Refining
Electron Backscattering Diffraction
spellingShingle Engineering::Mechanical engineering
Engineering::Materials
Grain Refining
Electron Backscattering Diffraction
Chen, Kewei
Huang, De Jun
Li, Hua
Jia, Ning
Chong, Warren
Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation
description In this study, the recrystallization process of selective laser melted (SLM) commercially pure titanium (CP-Ti) was followed by a quasi-in-situ electron backscatter diffraction (EBSD) method at 800 °C and 700 °C. Abnormal grain growth (AGG) initially emerges at the beginning of annealing at 800 °C and is primarily caused by strain-induced boundary migration (SIBM). However, at the beginning of annealing at 700 °C, many small equiaxed grains are formed due to more recrystallization nucleation, followed by the formation of AGG resulting from the secondary recrystallization. Based on these findings, appropriate control of the annealing time at 700 °C can mitigate AGG to obtain fine equiaxed grains with weak texture to enhance the tensile properties of SLM CP-Ti.
author2 School of Mechanical and Aerospace Engineering
author_facet School of Mechanical and Aerospace Engineering
Chen, Kewei
Huang, De Jun
Li, Hua
Jia, Ning
Chong, Warren
format Article
author Chen, Kewei
Huang, De Jun
Li, Hua
Jia, Ning
Chong, Warren
author_sort Chen, Kewei
title Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation
title_short Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation
title_full Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation
title_fullStr Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation
title_full_unstemmed Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation
title_sort avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation
publishDate 2022
url https://hdl.handle.net/10356/162543
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