Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation
In this study, the recrystallization process of selective laser melted (SLM) commercially pure titanium (CP-Ti) was followed by a quasi-in-situ electron backscatter diffraction (EBSD) method at 800 °C and 700 °C. Abnormal grain growth (AGG) initially emerges at the beginning of annealing at 800 °C a...
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sg-ntu-dr.10356-1625432022-10-28T07:35:35Z Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation Chen, Kewei Huang, De Jun Li, Hua Jia, Ning Chong, Warren School of Mechanical and Aerospace Engineering School of Materials Science and Engineering Singapore Centre for 3D Printing Engineering::Mechanical engineering Engineering::Materials Grain Refining Electron Backscattering Diffraction In this study, the recrystallization process of selective laser melted (SLM) commercially pure titanium (CP-Ti) was followed by a quasi-in-situ electron backscatter diffraction (EBSD) method at 800 °C and 700 °C. Abnormal grain growth (AGG) initially emerges at the beginning of annealing at 800 °C and is primarily caused by strain-induced boundary migration (SIBM). However, at the beginning of annealing at 700 °C, many small equiaxed grains are formed due to more recrystallization nucleation, followed by the formation of AGG resulting from the secondary recrystallization. Based on these findings, appropriate control of the annealing time at 700 °C can mitigate AGG to obtain fine equiaxed grains with weak texture to enhance the tensile properties of SLM CP-Ti. Economic Development Board (EDB) Nanyang Technological University This work is funded by the Economic Development Board Singapore, Nanyang Technological University, and Emerson Asia Pacific Pte Ltd. The authors acknowledge the use of electron microscopy and XRD equipment within the Facilities for Analysis, Characterization, Testing and Simulations (FACTS) at Nanyang Technological University 2022-10-28T07:35:35Z 2022-10-28T07:35:35Z 2022 Journal Article Chen, K., Huang, D. J., Li, H., Jia, N. & Chong, W. (2022). Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation. Scripta Materialia, 209, 114377-. https://dx.doi.org/10.1016/j.scriptamat.2021.114377 1359-6462 https://hdl.handle.net/10356/162543 10.1016/j.scriptamat.2021.114377 2-s2.0-85118542135 209 114377 en Scripta Materialia © 2021 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved. |
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Engineering::Mechanical engineering Engineering::Materials Grain Refining Electron Backscattering Diffraction Chen, Kewei Huang, De Jun Li, Hua Jia, Ning Chong, Warren Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation |
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In this study, the recrystallization process of selective laser melted (SLM) commercially pure titanium (CP-Ti) was followed by a quasi-in-situ electron backscatter diffraction (EBSD) method at 800 °C and 700 °C. Abnormal grain growth (AGG) initially emerges at the beginning of annealing at 800 °C and is primarily caused by strain-induced boundary migration (SIBM). However, at the beginning of annealing at 700 °C, many small equiaxed grains are formed due to more recrystallization nucleation, followed by the formation of AGG resulting from the secondary recrystallization. Based on these findings, appropriate control of the annealing time at 700 °C can mitigate AGG to obtain fine equiaxed grains with weak texture to enhance the tensile properties of SLM CP-Ti. |
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School of Mechanical and Aerospace Engineering |
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School of Mechanical and Aerospace Engineering Chen, Kewei Huang, De Jun Li, Hua Jia, Ning Chong, Warren |
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Article |
author |
Chen, Kewei Huang, De Jun Li, Hua Jia, Ning Chong, Warren |
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Chen, Kewei |
title |
Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation |
title_short |
Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation |
title_full |
Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation |
title_fullStr |
Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation |
title_full_unstemmed |
Avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation |
title_sort |
avoiding abnormal grain growth when annealing selective laser melted pure titanium by promoting nucleation |
publishDate |
2022 |
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https://hdl.handle.net/10356/162543 |
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1749179193536544768 |