Super hydrophobic SiO₂/phenolic resin-coated filter screen and its application in efficient oil–water separation

The discharge of industrial liquid waste continues to cause more and more environmental problems. The current research aims at developing a durable and highly efficient filter screen for oil-water separation. In this paper, hydrophobic nano-SiO2 and phenolic resin were used as raw materials. Hydroph...

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Main Authors: Zhao, Yan, Xiao, Zhongmin, Feng, Ziming, Luo, Qing, Liu, Xiaoping, Cui, Wei
Other Authors: School of Mechanical and Aerospace Engineering
Format: Article
Language:English
Published: 2023
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Online Access:https://hdl.handle.net/10356/168629
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Institution: Nanyang Technological University
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spelling sg-ntu-dr.10356-1686292023-06-17T16:47:56Z Super hydrophobic SiO₂/phenolic resin-coated filter screen and its application in efficient oil–water separation Zhao, Yan Xiao, Zhongmin Feng, Ziming Luo, Qing Liu, Xiaoping Cui, Wei School of Mechanical and Aerospace Engineering Engineering::Mechanical engineering Super Hydrophobic Coating Film The discharge of industrial liquid waste continues to cause more and more environmental problems. The current research aims at developing a durable and highly efficient filter screen for oil-water separation. In this paper, hydrophobic nano-SiO2 and phenolic resin were used as raw materials. Hydrophobic SiO2 particles were fixed on the surface of the coated filter screen by heating and curing the anchored particles. The surface morphology, element composition, surface roughness and water contact angle of the prepared super hydrophobic SiO2/phenolic resin-coated filter screen were analyzed and discussed by using SEM, EDS, AFM, OCA and other instruments. The results showed that the prepared filter screen contained Si, O, C elements, which proved that the resin coating film had adhered to the filter screen surface. When the aperture of the phenolic resin-coated filter screen was 400 meshes, the drainage angle reached a maximum value of 153.8° ± 0.8°. When two layers of hydrophobic SiO2 phenolic resin were coated on the screen, the surface of the filter screen had a sufficient nano-porous structure and high roughness. The tests showed that the minimum water contact angle of the filter screen exceeded 150°, which indicated excellent chemical resistance. Through the analysis of oil-water separation efficiency of isooctane, gasoline, n-hexane, dodecane, edible oil, dichloromethane and trichloromethane, it was concluded that the lowest separation efficiency for edible oil was 97.2%, and the highest separation efficiency for n-hexane was 99.4%. After 50 cycles of separation, the oil-water separation efficiency for n-hexane was still at 99%. Published version 2023-06-12T08:05:30Z 2023-06-12T08:05:30Z 2022 Journal Article Zhao, Y., Xiao, Z., Feng, Z., Luo, Q., Liu, X. & Cui, W. (2022). Super hydrophobic SiO₂/phenolic resin-coated filter screen and its application in efficient oil–water separation. Materials, 15(23), 8395-. https://dx.doi.org/10.3390/ma15238395 1996-1944 https://hdl.handle.net/10356/168629 10.3390/ma15238395 36499889 2-s2.0-85143804283 23 15 8395 en Materials © 2022 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https:// creativecommons.org/licenses/by/4.0/). application/pdf
institution Nanyang Technological University
building NTU Library
continent Asia
country Singapore
Singapore
content_provider NTU Library
collection DR-NTU
language English
topic Engineering::Mechanical engineering
Super Hydrophobic
Coating Film
spellingShingle Engineering::Mechanical engineering
Super Hydrophobic
Coating Film
Zhao, Yan
Xiao, Zhongmin
Feng, Ziming
Luo, Qing
Liu, Xiaoping
Cui, Wei
Super hydrophobic SiO₂/phenolic resin-coated filter screen and its application in efficient oil–water separation
description The discharge of industrial liquid waste continues to cause more and more environmental problems. The current research aims at developing a durable and highly efficient filter screen for oil-water separation. In this paper, hydrophobic nano-SiO2 and phenolic resin were used as raw materials. Hydrophobic SiO2 particles were fixed on the surface of the coated filter screen by heating and curing the anchored particles. The surface morphology, element composition, surface roughness and water contact angle of the prepared super hydrophobic SiO2/phenolic resin-coated filter screen were analyzed and discussed by using SEM, EDS, AFM, OCA and other instruments. The results showed that the prepared filter screen contained Si, O, C elements, which proved that the resin coating film had adhered to the filter screen surface. When the aperture of the phenolic resin-coated filter screen was 400 meshes, the drainage angle reached a maximum value of 153.8° ± 0.8°. When two layers of hydrophobic SiO2 phenolic resin were coated on the screen, the surface of the filter screen had a sufficient nano-porous structure and high roughness. The tests showed that the minimum water contact angle of the filter screen exceeded 150°, which indicated excellent chemical resistance. Through the analysis of oil-water separation efficiency of isooctane, gasoline, n-hexane, dodecane, edible oil, dichloromethane and trichloromethane, it was concluded that the lowest separation efficiency for edible oil was 97.2%, and the highest separation efficiency for n-hexane was 99.4%. After 50 cycles of separation, the oil-water separation efficiency for n-hexane was still at 99%.
author2 School of Mechanical and Aerospace Engineering
author_facet School of Mechanical and Aerospace Engineering
Zhao, Yan
Xiao, Zhongmin
Feng, Ziming
Luo, Qing
Liu, Xiaoping
Cui, Wei
format Article
author Zhao, Yan
Xiao, Zhongmin
Feng, Ziming
Luo, Qing
Liu, Xiaoping
Cui, Wei
author_sort Zhao, Yan
title Super hydrophobic SiO₂/phenolic resin-coated filter screen and its application in efficient oil–water separation
title_short Super hydrophobic SiO₂/phenolic resin-coated filter screen and its application in efficient oil–water separation
title_full Super hydrophobic SiO₂/phenolic resin-coated filter screen and its application in efficient oil–water separation
title_fullStr Super hydrophobic SiO₂/phenolic resin-coated filter screen and its application in efficient oil–water separation
title_full_unstemmed Super hydrophobic SiO₂/phenolic resin-coated filter screen and its application in efficient oil–water separation
title_sort super hydrophobic sio₂/phenolic resin-coated filter screen and its application in efficient oil–water separation
publishDate 2023
url https://hdl.handle.net/10356/168629
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