Microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316L-Inconel 718 alloy fabricated by laser powder bed fusion

The microstructures and the mechanical properties of a laser powder bed fusion manufactured compositionally graded alloy of the austenitic stainless steel 316L and Inconel 718, in the as-built and heat-treated conditions, were investigated. In all the cross sections of the as-built compositionally g...

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Main Authors: Wen, Yaojie, Gao, Jianbao, Narayan, Ramasubramanian Lakshmi, Wang, Pei, Zhang, Lijun, Zhang, Baicheng, Ramamurty, Upadrasta, Qu, Xuanhui
Other Authors: School of Mechanical and Aerospace Engineering
Format: Article
Language:English
Published: 2023
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Online Access:https://hdl.handle.net/10356/172803
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spelling sg-ntu-dr.10356-1728032023-12-20T08:10:45Z Microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316L-Inconel 718 alloy fabricated by laser powder bed fusion Wen, Yaojie Gao, Jianbao Narayan, Ramasubramanian Lakshmi Wang, Pei Zhang, Lijun Zhang, Baicheng Ramamurty, Upadrasta Qu, Xuanhui School of Mechanical and Aerospace Engineering Institute of Materials Research and Engineering Engineering::Materials Engineering::Mechanical engineering Laser Powder Bed Fusion Compositionally Graded Alloys The microstructures and the mechanical properties of a laser powder bed fusion manufactured compositionally graded alloy of the austenitic stainless steel 316L and Inconel 718, in the as-built and heat-treated conditions, were investigated. In all the cross sections of the as-built compositionally graded alloy, along the compositional gradient direction, which is perpendicular to the build direction, the microstructure primarily consists of sub-micron sized cells embedded within <001> textured columnar grains of the γ phase along with Laves phases at their grain boundaries. Heat treatment, which involves solutionizing at 1040 °C for 1 h followed by annealing at 720 °C and 620 °C for 10 h each, leads to coarsening of Laves phases, slight modification in texture and the annihilation of the sub-grain structure of the compositionally graded alloy, but does not alter the columnar grain size. It also leads to precipitation of the γ" and γ' phases in the portions of the compositionally graded alloy with >70 wt% of IN718. The hardness, yield strength and tensile strength of the compositionally graded alloy increase but ductility decreases from the SS316L-rich end to the IN718-rich end along the gradient direction. Heat treatment smoothens the variations in YS and UTS along the gradient direction in cross sections with <82 wt% IN718 but reduces their relative magnitude compared to that of the as-built condition. The heat-treated compositionally graded alloy exhibits significantly higher YS and UTS but lower ductility than that in the as-built condition, in portions with ≥82 wt% IN718. These mechanical property variations are analyzed in detail by considering variations in the composition, microstructural features, and contents of different phases in the as-built and heat-treated compositionally graded alloy. Finally, an appraisal on the appropriate compositional gradient and utility of the heat treatment of the compositionally graded alloy is discussed in the context of specific requirements in structural applications. Agency for Science, Technology and Research (A*STAR) The authors acknowledge the financial support of the National Key R&D Program of China (2021YFB38002300), National Natural Science Foundation of China (No.: 52171026, 51901020). RLN’s research at IITD was supported through the Start-up research grant (No. SRG/2020/ 000095) of Science and Engineering Research Board, DST, GoI. Research at NTU was supported by the Structural Metal Alloys Program (Grant Ref. No. A18b1B0061) of the Agency for Science, Technology and Research of Singapore. Research at IMRE was supported by the AME (IRG) Thematic Grant Call on Cleaner Manufacturing, grant No. A20E7c0109, in Agency for Science, Technology and Research in Singapore. 2023-12-20T07:31:10Z 2023-12-20T07:31:10Z 2023 Journal Article Wen, Y., Gao, J., Narayan, R. L., Wang, P., Zhang, L., Zhang, B., Ramamurty, U. & Qu, X. (2023). Microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316L-Inconel 718 alloy fabricated by laser powder bed fusion. Materials Science and Engineering A, 862, 144515-. https://dx.doi.org/10.1016/j.msea.2022.144515 0921-5093 https://hdl.handle.net/10356/172803 10.1016/j.msea.2022.144515 2-s2.0-85145647943 862 144515 en A18B1b0061 Materials Science and Engineering A © 2022 Elsevier B.V. All rights reserved.
institution Nanyang Technological University
building NTU Library
continent Asia
country Singapore
Singapore
content_provider NTU Library
collection DR-NTU
language English
topic Engineering::Materials
Engineering::Mechanical engineering
Laser Powder Bed Fusion
Compositionally Graded Alloys
spellingShingle Engineering::Materials
Engineering::Mechanical engineering
Laser Powder Bed Fusion
Compositionally Graded Alloys
Wen, Yaojie
Gao, Jianbao
Narayan, Ramasubramanian Lakshmi
Wang, Pei
Zhang, Lijun
Zhang, Baicheng
Ramamurty, Upadrasta
Qu, Xuanhui
Microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316L-Inconel 718 alloy fabricated by laser powder bed fusion
description The microstructures and the mechanical properties of a laser powder bed fusion manufactured compositionally graded alloy of the austenitic stainless steel 316L and Inconel 718, in the as-built and heat-treated conditions, were investigated. In all the cross sections of the as-built compositionally graded alloy, along the compositional gradient direction, which is perpendicular to the build direction, the microstructure primarily consists of sub-micron sized cells embedded within <001> textured columnar grains of the γ phase along with Laves phases at their grain boundaries. Heat treatment, which involves solutionizing at 1040 °C for 1 h followed by annealing at 720 °C and 620 °C for 10 h each, leads to coarsening of Laves phases, slight modification in texture and the annihilation of the sub-grain structure of the compositionally graded alloy, but does not alter the columnar grain size. It also leads to precipitation of the γ" and γ' phases in the portions of the compositionally graded alloy with >70 wt% of IN718. The hardness, yield strength and tensile strength of the compositionally graded alloy increase but ductility decreases from the SS316L-rich end to the IN718-rich end along the gradient direction. Heat treatment smoothens the variations in YS and UTS along the gradient direction in cross sections with <82 wt% IN718 but reduces their relative magnitude compared to that of the as-built condition. The heat-treated compositionally graded alloy exhibits significantly higher YS and UTS but lower ductility than that in the as-built condition, in portions with ≥82 wt% IN718. These mechanical property variations are analyzed in detail by considering variations in the composition, microstructural features, and contents of different phases in the as-built and heat-treated compositionally graded alloy. Finally, an appraisal on the appropriate compositional gradient and utility of the heat treatment of the compositionally graded alloy is discussed in the context of specific requirements in structural applications.
author2 School of Mechanical and Aerospace Engineering
author_facet School of Mechanical and Aerospace Engineering
Wen, Yaojie
Gao, Jianbao
Narayan, Ramasubramanian Lakshmi
Wang, Pei
Zhang, Lijun
Zhang, Baicheng
Ramamurty, Upadrasta
Qu, Xuanhui
format Article
author Wen, Yaojie
Gao, Jianbao
Narayan, Ramasubramanian Lakshmi
Wang, Pei
Zhang, Lijun
Zhang, Baicheng
Ramamurty, Upadrasta
Qu, Xuanhui
author_sort Wen, Yaojie
title Microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316L-Inconel 718 alloy fabricated by laser powder bed fusion
title_short Microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316L-Inconel 718 alloy fabricated by laser powder bed fusion
title_full Microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316L-Inconel 718 alloy fabricated by laser powder bed fusion
title_fullStr Microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316L-Inconel 718 alloy fabricated by laser powder bed fusion
title_full_unstemmed Microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316L-Inconel 718 alloy fabricated by laser powder bed fusion
title_sort microstructure-property correlations in as-built and heat-treated compositionally graded stainless steel 316l-inconel 718 alloy fabricated by laser powder bed fusion
publishDate 2023
url https://hdl.handle.net/10356/172803
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