Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer

Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer

Electrochemical in operando X-ray diffraction (XRD) is a powerful method to analyze structural changes of energy storage materials while inserting/de-inserting charge carriers, such as Li- or Na-ions, into/from a host structure. The design of an XRD in operando cell is presented, which enables the u...

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Main Authors: Hartung, Steffen, Bucher, Nicolas, Bucher, Ramona, Srinivasan, Madhavi
Other Authors: School of Materials Science & Engineering
Format: Article
Language:English
Published: 2015
Subjects:
X-ray diffraction
Online Access:https://hdl.handle.net/10356/81215
http://hdl.handle.net/10220/39169
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Institution: Nanyang Technological University
Language: English
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spelling sg-ntu-dr.10356-812152023-07-14T15:50:18Z Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer Hartung, Steffen Bucher, Nicolas Bucher, Ramona Srinivasan, Madhavi School of Materials Science & Engineering X-ray diffraction Electrochemical in operando X-ray diffraction (XRD) is a powerful method to analyze structural changes of energy storage materials while inserting/de-inserting charge carriers, such as Li- or Na-ions, into/from a host structure. The design of an XRD in operando cell is presented, which enables the use of thin (6 μm) aluminum foil as X-ray window as a non-toxic alternative to conventional beryllium windows. Owing to the reduced thickness, diffraction patterns and their changes during cycling can be observed with excellent quality, which was demonstrated for two cathode materials for sodium-ion batteries in a half-cell set-up, P2-Na0.7MnO2 and Na2.55V6O16⋅0.6H2O. NRF (Natl Research Foundation, S’pore) Published version 2015-12-18T06:59:47Z 2019-12-06T14:23:50Z 2015-12-18T06:59:47Z 2019-12-06T14:23:50Z 2015 Journal Article Hartung, S., Bucher, N., Bucher, R., & Srinivasan, M. (2015). Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer. Review of Scientific Instruments, 86(8), 086102-. 0034-6748 https://hdl.handle.net/10356/81215 http://hdl.handle.net/10220/39169 10.1063/1.4926465 en Review of Scientific Instruments © 2015 AIP Publishing LLC. This paper was published in Review of Scientific Instruments and is made available as an electronic reprint (preprint) with permission of AIP Publishing LLC. The paper can be found at the following official DOI: [http://dx.doi.org/10.1063/1.4926465]. One print or electronic copy may be made for personal use only. Systematic or multiple reproduction, distribution to multiple locations via electronic or other means, duplication of any material in this paper for a fee or for commercial purposes, or modification of the content of the paper is prohibited and is subject to penalties under law. 3 p. application/pdf
institution Nanyang Technological University
building NTU Library
continent Asia
country Singapore
Singapore
content_provider NTU Library
collection DR-NTU
language English
topic X-ray diffraction
spellingShingle X-ray diffraction
Hartung, Steffen
Bucher, Nicolas
Bucher, Ramona
Srinivasan, Madhavi
Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer
description Electrochemical in operando X-ray diffraction (XRD) is a powerful method to analyze structural changes of energy storage materials while inserting/de-inserting charge carriers, such as Li- or Na-ions, into/from a host structure. The design of an XRD in operando cell is presented, which enables the use of thin (6 μm) aluminum foil as X-ray window as a non-toxic alternative to conventional beryllium windows. Owing to the reduced thickness, diffraction patterns and their changes during cycling can be observed with excellent quality, which was demonstrated for two cathode materials for sodium-ion batteries in a half-cell set-up, P2-Na0.7MnO2 and Na2.55V6O16⋅0.6H2O.
author2 School of Materials Science & Engineering
author_facet School of Materials Science & Engineering
Hartung, Steffen
Bucher, Nicolas
Bucher, Ramona
Srinivasan, Madhavi
format Article
author Hartung, Steffen
Bucher, Nicolas
Bucher, Ramona
Srinivasan, Madhavi
author_sort Hartung, Steffen
title Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer
title_short Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer
title_full Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer
title_fullStr Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer
title_full_unstemmed Note: Electrochemical cell for in operando X-ray diffraction measurements on a conventional X-ray diffractometer
title_sort note: electrochemical cell for in operando x-ray diffraction measurements on a conventional x-ray diffractometer
publishDate 2015
url https://hdl.handle.net/10356/81215
http://hdl.handle.net/10220/39169
_version_ 1772828168577613824

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