Synthesis of cubic CuFe<inf>2</inf>O<inf>4</inf> nanoparticles by microwave-hydrothermal method and their magnetic properties
© 2016 Elsevier B.V. All rights reserved. Copper ferrite (CuFe 2 O 4 ) nanoparticles were prepared in alkaline solutions containing Cu(NO 3 ) 2 ·6H 2 O and Fe(NO 3 ) 3 ·9H 2 O with the pH of 6-12 by microwave-hydrothermal method. The as-prepared products characterized by XRD were specified as cubic...
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Main Authors: | , , , |
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Format: | Journal |
Published: |
2017
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Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84953438703&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/42014 |
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Institution: | Chiang Mai University |
Summary: | © 2016 Elsevier B.V. All rights reserved. Copper ferrite (CuFe 2 O 4 ) nanoparticles were prepared in alkaline solutions containing Cu(NO 3 ) 2 ·6H 2 O and Fe(NO 3 ) 3 ·9H 2 O with the pH of 6-12 by microwave-hydrothermal method. The as-prepared products characterized by XRD were specified as cubic CuFe 2 O 4 phase. Average sizes of the CuFe 2 O 4 nanoparticles calculated by Scherrer formula are in the same range as those obtained by TEM analysis. FTIR shows main transmittance band at 585 cm -1 , corresponding to stretching mode of tetrahedral complexes. Saturation magnetization, remanence and coercivity were increased with increasing in the particle-size and crystalline degree of the nanoparticles. |
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