Facile and efficient synthesis of C<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation

Facile and efficient synthesis of C<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation

© 2014 Elsevier Ltd. All rights reserved. A rapid and efficient method for preparation of C 2 -symmetrical 1,3,5-triazine polycarboxylate ligands was developed. The reactions included either selective mono- or di-substitution of 2,4,6-trichloro-1,3,5-triazine with various nucleophiles containing car...

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Main Authors: Watcharee Funfuenha, Wong Phakhodee, Mookda Pattarawarapan
Format: Journal
Published: 2018
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84949124339&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/44971
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-449712018-01-24T06:02:14Z Facile and efficient synthesis of C<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation Watcharee Funfuenha Wong Phakhodee Mookda Pattarawarapan © 2014 Elsevier Ltd. All rights reserved. A rapid and efficient method for preparation of C 2 -symmetrical 1,3,5-triazine polycarboxylate ligands was developed. The reactions included either selective mono- or di-substitution of 2,4,6-trichloro-1,3,5-triazine with various nucleophiles containing carboxyl group(s), followed by nucleophilic displacement of the remained chloride(s) in aqueous media under microwave irradiation. Novel C 2 -symmetrical tripodal ligands were afforded in good yields and purities under short reaction time with simple work-up, which are potentially useful as structural directing units in metal-organic frameworks. 2018-01-24T06:02:14Z 2018-01-24T06:02:14Z 2014-09-02 Journal 14645416 00404020 2-s2.0-84949124339 10.1016/j.tet.2014.06.127 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84949124339&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/44971
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
description © 2014 Elsevier Ltd. All rights reserved. A rapid and efficient method for preparation of C 2 -symmetrical 1,3,5-triazine polycarboxylate ligands was developed. The reactions included either selective mono- or di-substitution of 2,4,6-trichloro-1,3,5-triazine with various nucleophiles containing carboxyl group(s), followed by nucleophilic displacement of the remained chloride(s) in aqueous media under microwave irradiation. Novel C 2 -symmetrical tripodal ligands were afforded in good yields and purities under short reaction time with simple work-up, which are potentially useful as structural directing units in metal-organic frameworks.
format Journal
author Watcharee Funfuenha
Wong Phakhodee
Mookda Pattarawarapan
spellingShingle Watcharee Funfuenha
Wong Phakhodee
Mookda Pattarawarapan
Facile and efficient synthesis of C<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation
author_facet Watcharee Funfuenha
Wong Phakhodee
Mookda Pattarawarapan
author_sort Watcharee Funfuenha
title Facile and efficient synthesis of C<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation
title_short Facile and efficient synthesis of C<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation
title_full Facile and efficient synthesis of C<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation
title_fullStr Facile and efficient synthesis of C<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation
title_full_unstemmed Facile and efficient synthesis of C<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation
title_sort facile and efficient synthesis of c<inf>2</inf>-symmetrical 1,3,5-triazine polycarboxylate ligands under microwave irradiation
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84949124339&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/44971
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