Synthesis of CdIn<inf>2</inf>Se<inf>4</inf>and Cu<inf>0.5</inf>Ag<inf>1.5</inf>InSe<inf>3</inf>compounds via chemical and solid-State methods

CdIn 2 Se 4 and Cu 0.5 Ag 1.5 InSe 3 are high-performance thermoelectric materials. In this study, both CdIn 2 Se 4 and Cu 0.5 Ag 1.5 InSe 3 powders were synthesized using a microwave and solution method followed by annealing in nitrogen atmosphere. CdIn 2 Se 4 was synthesized by two routes. First,...

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Main Authors: Viratchara Laokawee, Thapanee Sarakonsri, Chanchana Thanachayanont
Format: Journal
Published: 2018
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84899099067&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/45549
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-455492018-01-24T06:12:06Z Synthesis of CdIn<inf>2</inf>Se<inf>4</inf>and Cu<inf>0.5</inf>Ag<inf>1.5</inf>InSe<inf>3</inf>compounds via chemical and solid-State methods Viratchara Laokawee Thapanee Sarakonsri Chanchana Thanachayanont CdIn 2 Se 4 and Cu 0.5 Ag 1.5 InSe 3 are high-performance thermoelectric materials. In this study, both CdIn 2 Se 4 and Cu 0.5 Ag 1.5 InSe 3 powders were synthesized using a microwave and solution method followed by annealing in nitrogen atmosphere. CdIn 2 Se 4 was synthesized by two routes. First, CdSe was prepared using a microwave method. Second, In metal was prepared using a solution method. The prepared metals were annealed in nitrogen atmosphere. From the x-ray diffraction (XRD) results, CdIn 2 Se 4 was observed as the main phase with CdSe and In 2 O 3 as contaminant phases. The synthesis of Cu 0.5 Ag 1.5 InSe 3 was also divided into two steps. First, CuAg and Se were prepared using a microwave method. Second, In metal was prepared using a solution method. The prepared metals were annealed in nitrogen atmosphere. From the XRD results, Cu 0.5 Ag 1.5 InSe 3 was observed as the main phase with Cu 0.5-x Ag 1.5-y In x+y Se and Se as contaminant phases. © 2014 TMS. 2018-01-24T06:12:06Z 2018-01-24T06:12:06Z 2014-01-01 Journal 03615235 2-s2.0-84899099067 10.1007/s11664-013-2961-9 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84899099067&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/45549
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
description CdIn 2 Se 4 and Cu 0.5 Ag 1.5 InSe 3 are high-performance thermoelectric materials. In this study, both CdIn 2 Se 4 and Cu 0.5 Ag 1.5 InSe 3 powders were synthesized using a microwave and solution method followed by annealing in nitrogen atmosphere. CdIn 2 Se 4 was synthesized by two routes. First, CdSe was prepared using a microwave method. Second, In metal was prepared using a solution method. The prepared metals were annealed in nitrogen atmosphere. From the x-ray diffraction (XRD) results, CdIn 2 Se 4 was observed as the main phase with CdSe and In 2 O 3 as contaminant phases. The synthesis of Cu 0.5 Ag 1.5 InSe 3 was also divided into two steps. First, CuAg and Se were prepared using a microwave method. Second, In metal was prepared using a solution method. The prepared metals were annealed in nitrogen atmosphere. From the XRD results, Cu 0.5 Ag 1.5 InSe 3 was observed as the main phase with Cu 0.5-x Ag 1.5-y In x+y Se and Se as contaminant phases. © 2014 TMS.
format Journal
author Viratchara Laokawee
Thapanee Sarakonsri
Chanchana Thanachayanont
spellingShingle Viratchara Laokawee
Thapanee Sarakonsri
Chanchana Thanachayanont
Synthesis of CdIn<inf>2</inf>Se<inf>4</inf>and Cu<inf>0.5</inf>Ag<inf>1.5</inf>InSe<inf>3</inf>compounds via chemical and solid-State methods
author_facet Viratchara Laokawee
Thapanee Sarakonsri
Chanchana Thanachayanont
author_sort Viratchara Laokawee
title Synthesis of CdIn<inf>2</inf>Se<inf>4</inf>and Cu<inf>0.5</inf>Ag<inf>1.5</inf>InSe<inf>3</inf>compounds via chemical and solid-State methods
title_short Synthesis of CdIn<inf>2</inf>Se<inf>4</inf>and Cu<inf>0.5</inf>Ag<inf>1.5</inf>InSe<inf>3</inf>compounds via chemical and solid-State methods
title_full Synthesis of CdIn<inf>2</inf>Se<inf>4</inf>and Cu<inf>0.5</inf>Ag<inf>1.5</inf>InSe<inf>3</inf>compounds via chemical and solid-State methods
title_fullStr Synthesis of CdIn<inf>2</inf>Se<inf>4</inf>and Cu<inf>0.5</inf>Ag<inf>1.5</inf>InSe<inf>3</inf>compounds via chemical and solid-State methods
title_full_unstemmed Synthesis of CdIn<inf>2</inf>Se<inf>4</inf>and Cu<inf>0.5</inf>Ag<inf>1.5</inf>InSe<inf>3</inf>compounds via chemical and solid-State methods
title_sort synthesis of cdin<inf>2</inf>se<inf>4</inf>and cu<inf>0.5</inf>ag<inf>1.5</inf>inse<inf>3</inf>compounds via chemical and solid-state methods
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84899099067&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/45549
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