Effect of composition on phase formation, microstructure and dielectric properties of sol-bonded PZTN-PZT ceramics
The PZTN sol-powder was synthesized from a triol sol-gel process, while the ball milled PZT powder prepared from the reagent grade oxides of PbO, ZrO 2 and TiO 2 powders. The sol and balled milled powders were mixed at a ratio of 30:70, 50:50 and 70:30 by weight. The results showed that at a composi...
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| Main Authors: | , , |
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| Format: | Journal |
| Published: |
2018
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| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84891816286&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/47422 |
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| Institution: | Chiang Mai University |
| Summary: | The PZTN sol-powder was synthesized from a triol sol-gel process, while the ball milled PZT powder prepared from the reagent grade oxides of PbO, ZrO 2 and TiO 2 powders. The sol and balled milled powders were mixed at a ratio of 30:70, 50:50 and 70:30 by weight. The results showed that at a composition of 70:30 had the maximum density values compared with the other two compositions. X-ray diffraction analysis indicated that a single tetragonal phase was observed at all sintering temperatures for this composition (70:30). The maximum room temperature dielectric constant measured at 1 kHz was 1151 could be achieved for the ceramic sintered at 1100°C for 4 h, where the densification was optimized. © 2013 Copyright Taylor and Francis Group, LLC. |
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