Synthesis of coral-like, straw-tied-like, and flower-like antimony sulfides by a facile wet-chemical method
Antimony sulfide (Sb 2 S 3 ) was successfully synthesized from antimony chloride (SbCl 3 ) and sodium thiosulfate pentahydrate (Na 2 S 2 O 3 ·5H 2 O) in ethylene glycol (EG) without using any template by a facile wet-chemical method. X-ray diffraction (XRD), scanning electron microscopy (SEM), and t...
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| Main Authors: | , , , |
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| Format: | Journal |
| Published: |
2018
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| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84881411465&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/47718 |
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| Institution: | Chiang Mai University |
| Summary: | Antimony sulfide (Sb 2 S 3 ) was successfully synthesized from antimony chloride (SbCl 3 ) and sodium thiosulfate pentahydrate (Na 2 S 2 O 3 ·5H 2 O) in ethylene glycol (EG) without using any template by a facile wet-chemical method. X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) show that the products were orthorhombic Sb 2 S 3 nanorods forming the coral-like, straw-tied-like, and flower-like architectures with the nanorods growing along the [001] direction. The energy gap (E g) was determined by UV-visible absorption to be 1.52 eV. © 2013 Jutarat Kavinchan et al. |
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