Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
xPb(Zr1/ 2 Ti1/ 2 )O 3 -(1-x)Pb(Zn1/ 3 Nb2/ 3 )O 3 or xPZT-(1-x)PZN (x = 0.85-0.95)powders were prepared by a modified mixed-oxide synthetic route via a combination of Zn 2 Nb 34 O 87 precursor and rapid vibro-milling techniques. Effects of calcination temperature on phase formation, morphology, par...
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th-cmuir.6653943832-482152018-04-25T08:49:12Z Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders Penphitcha Amonpattaratkit Supon Ananta xPb(Zr1/ 2 Ti1/ 2 )O 3 -(1-x)Pb(Zn1/ 3 Nb2/ 3 )O 3 or xPZT-(1-x)PZN (x = 0.85-0.95)powders were prepared by a modified mixed-oxide synthetic route via a combination of Zn 2 Nb 34 O 87 precursor and rapid vibro-milling techniques. Effects of calcination temperature on phase formation, morphology, particle size and chemical composition of perovskite ferroelectric powders in the solid solution of PZT-PZN system were investigated. Perovskite phase transition from a tetragonal to a coexistence of tetragonal and rhombohedral phases occurred as composition and firing temperature change. The tetragonality factor and degree of spherical grain shape were observed to increase with increasing PZT content. Moreover, the degree of agglomeration and averaged particle size of the PZT-PZN powders were also found to increase at higher calcination temperatures. © 2013 Copyright Taylor and Francis Group, LLC. 2018-04-25T08:49:12Z 2018-04-25T08:49:12Z 2013-01-01 Journal 15635112 00150193 2-s2.0-84891821328 10.1080/00150193.2013.846128 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84891821328&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/48215 |
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xPb(Zr1/ 2 Ti1/ 2 )O 3 -(1-x)Pb(Zn1/ 3 Nb2/ 3 )O 3 or xPZT-(1-x)PZN (x = 0.85-0.95)powders were prepared by a modified mixed-oxide synthetic route via a combination of Zn 2 Nb 34 O 87 precursor and rapid vibro-milling techniques. Effects of calcination temperature on phase formation, morphology, particle size and chemical composition of perovskite ferroelectric powders in the solid solution of PZT-PZN system were investigated. Perovskite phase transition from a tetragonal to a coexistence of tetragonal and rhombohedral phases occurred as composition and firing temperature change. The tetragonality factor and degree of spherical grain shape were observed to increase with increasing PZT content. Moreover, the degree of agglomeration and averaged particle size of the PZT-PZN powders were also found to increase at higher calcination temperatures. © 2013 Copyright Taylor and Francis Group, LLC. |
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Penphitcha Amonpattaratkit Supon Ananta |
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Penphitcha Amonpattaratkit Supon Ananta Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders |
author_facet |
Penphitcha Amonpattaratkit Supon Ananta |
author_sort |
Penphitcha Amonpattaratkit |
title |
Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders |
title_short |
Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders |
title_full |
Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders |
title_fullStr |
Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders |
title_full_unstemmed |
Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders |
title_sort |
synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders |
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2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84891821328&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/48215 |
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