Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders

xPb(Zr1/ 2 Ti1/ 2 )O 3 -(1-x)Pb(Zn1/ 3 Nb2/ 3 )O 3 or xPZT-(1-x)PZN (x = 0.85-0.95)powders were prepared by a modified mixed-oxide synthetic route via a combination of Zn 2 Nb 34 O 87 precursor and rapid vibro-milling techniques. Effects of calcination temperature on phase formation, morphology, par...

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Main Authors: Penphitcha Amonpattaratkit, Supon Ananta
Format: Journal
Published: 2018
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84891821328&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/48215
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-482152018-04-25T08:49:12Z Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders Penphitcha Amonpattaratkit Supon Ananta xPb(Zr1/ 2 Ti1/ 2 )O 3 -(1-x)Pb(Zn1/ 3 Nb2/ 3 )O 3 or xPZT-(1-x)PZN (x = 0.85-0.95)powders were prepared by a modified mixed-oxide synthetic route via a combination of Zn 2 Nb 34 O 87 precursor and rapid vibro-milling techniques. Effects of calcination temperature on phase formation, morphology, particle size and chemical composition of perovskite ferroelectric powders in the solid solution of PZT-PZN system were investigated. Perovskite phase transition from a tetragonal to a coexistence of tetragonal and rhombohedral phases occurred as composition and firing temperature change. The tetragonality factor and degree of spherical grain shape were observed to increase with increasing PZT content. Moreover, the degree of agglomeration and averaged particle size of the PZT-PZN powders were also found to increase at higher calcination temperatures. © 2013 Copyright Taylor and Francis Group, LLC. 2018-04-25T08:49:12Z 2018-04-25T08:49:12Z 2013-01-01 Journal 15635112 00150193 2-s2.0-84891821328 10.1080/00150193.2013.846128 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84891821328&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/48215
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
description xPb(Zr1/ 2 Ti1/ 2 )O 3 -(1-x)Pb(Zn1/ 3 Nb2/ 3 )O 3 or xPZT-(1-x)PZN (x = 0.85-0.95)powders were prepared by a modified mixed-oxide synthetic route via a combination of Zn 2 Nb 34 O 87 precursor and rapid vibro-milling techniques. Effects of calcination temperature on phase formation, morphology, particle size and chemical composition of perovskite ferroelectric powders in the solid solution of PZT-PZN system were investigated. Perovskite phase transition from a tetragonal to a coexistence of tetragonal and rhombohedral phases occurred as composition and firing temperature change. The tetragonality factor and degree of spherical grain shape were observed to increase with increasing PZT content. Moreover, the degree of agglomeration and averaged particle size of the PZT-PZN powders were also found to increase at higher calcination temperatures. © 2013 Copyright Taylor and Francis Group, LLC.
format Journal
author Penphitcha Amonpattaratkit
Supon Ananta
spellingShingle Penphitcha Amonpattaratkit
Supon Ananta
Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
author_facet Penphitcha Amonpattaratkit
Supon Ananta
author_sort Penphitcha Amonpattaratkit
title Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_short Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_full Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_fullStr Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_full_unstemmed Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_sort synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84891821328&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/48215
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