Phase and chemical characterization of perovskite nickel niobate ceramics fabricated via a precursor method

Perovskite relaxor ferroelectric lead nickel niobate (PNN) ceramics were fabricated by using B-site precursor method, in which columbite-NiNb 2O6 was employed as key precursor. It has been found that optimization of sintering condition can successfully lead to highly dense PNN ceramics. Although XRD...

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Main Authors: Laongnuan Srisombat, Orawan Khamman, Rattikorn Yimnirun, S. Supon Ananta, T. Randall Lee
Format: Journal
Published: 2018
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http://cmuir.cmu.ac.th/jspui/handle/6653943832/48922
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-489222018-08-16T02:18:40Z Phase and chemical characterization of perovskite nickel niobate ceramics fabricated via a precursor method Laongnuan Srisombat Orawan Khamman Rattikorn Yimnirun S. Supon Ananta T. Randall Lee Biochemistry, Genetics and Molecular Biology Chemistry Materials Science Mathematics Physics and Astronomy Perovskite relaxor ferroelectric lead nickel niobate (PNN) ceramics were fabricated by using B-site precursor method, in which columbite-NiNb 2O6 was employed as key precursor. It has been found that optimization of sintering condition can successfully lead to highly dense PNN ceramics. Although XRD analysis revealed that the ceramics consist of pure perovskite phase, significant fluctuation in chemical composition, precipitation of unreacted precursor and the formation of unwanted phases were found via a combination between SEM EDX and XPS techniques. 2018-08-16T02:06:42Z 2018-08-16T02:06:42Z 2009-01-01 Journal 01252526 2-s2.0-67650505597 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=67650505597&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/48922
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Biochemistry, Genetics and Molecular Biology
Chemistry
Materials Science
Mathematics
Physics and Astronomy
spellingShingle Biochemistry, Genetics and Molecular Biology
Chemistry
Materials Science
Mathematics
Physics and Astronomy
Laongnuan Srisombat
Orawan Khamman
Rattikorn Yimnirun
S. Supon Ananta
T. Randall Lee
Phase and chemical characterization of perovskite nickel niobate ceramics fabricated via a precursor method
description Perovskite relaxor ferroelectric lead nickel niobate (PNN) ceramics were fabricated by using B-site precursor method, in which columbite-NiNb 2O6 was employed as key precursor. It has been found that optimization of sintering condition can successfully lead to highly dense PNN ceramics. Although XRD analysis revealed that the ceramics consist of pure perovskite phase, significant fluctuation in chemical composition, precipitation of unreacted precursor and the formation of unwanted phases were found via a combination between SEM EDX and XPS techniques.
format Journal
author Laongnuan Srisombat
Orawan Khamman
Rattikorn Yimnirun
S. Supon Ananta
T. Randall Lee
author_facet Laongnuan Srisombat
Orawan Khamman
Rattikorn Yimnirun
S. Supon Ananta
T. Randall Lee
author_sort Laongnuan Srisombat
title Phase and chemical characterization of perovskite nickel niobate ceramics fabricated via a precursor method
title_short Phase and chemical characterization of perovskite nickel niobate ceramics fabricated via a precursor method
title_full Phase and chemical characterization of perovskite nickel niobate ceramics fabricated via a precursor method
title_fullStr Phase and chemical characterization of perovskite nickel niobate ceramics fabricated via a precursor method
title_full_unstemmed Phase and chemical characterization of perovskite nickel niobate ceramics fabricated via a precursor method
title_sort phase and chemical characterization of perovskite nickel niobate ceramics fabricated via a precursor method
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=67650505597&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/48922
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