Preparation, characterization and photoluminescence of nanocrystalline calcium molybdate
Nanocrystalline calcium molybdate was successfully synthesized from Ca(NO 3) 2 and Na 2MoO 4 in ethylene glycol using a microwave radiation method. Body-centered tetragonal structured calcium molybdate with n...
Saved in:
Main Authors: | , , |
---|---|
Format: | Journal |
Published: |
2018
|
Subjects: | |
Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=67649270499&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/49082 |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
Institution: | Chiang Mai University |
id |
th-cmuir.6653943832-49082 |
---|---|
record_format |
dspace |
spelling |
th-cmuir.6653943832-490822018-08-16T02:11:51Z Preparation, characterization and photoluminescence of nanocrystalline calcium molybdate Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Engineering Materials Science Nanocrystalline calcium molybdate was successfully synthesized from Ca(NO 3) 2 and Na 2MoO 4 in ethylene glycol using a microwave radiation method. Body-centered tetragonal structured calcium molybdate with narrow nanosized distribution was detected using XRD, SAED and TEM. A diffraction pattern was also simulated and was found to be in accordance with those obtained from the experiment and JCPDS standard. Raman and FTIR spectra show the Mo-O prominent stretching bands in the [MoO 4] 2- tetrahedrons at 879.59 and 743-895 cm -1, respectively. Photoluminescence emission of CaMoO 4 was detected at 477 nm, caused by the annihilation of a self-trapped excitons from the [MoO 4] 2- excited complex. © 2009 Elsevier B.V. All rights reserved. 2018-08-16T02:09:34Z 2018-08-16T02:09:34Z 2009-07-29 Journal 09258388 2-s2.0-67649270499 10.1016/j.jallcom.2009.03.037 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=67649270499&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/49082 |
institution |
Chiang Mai University |
building |
Chiang Mai University Library |
country |
Thailand |
collection |
CMU Intellectual Repository |
topic |
Engineering Materials Science |
spellingShingle |
Engineering Materials Science Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Preparation, characterization and photoluminescence of nanocrystalline calcium molybdate |
description |
Nanocrystalline calcium molybdate was successfully synthesized from Ca(NO 3) 2 and Na 2MoO 4 in ethylene glycol using a microwave radiation method. Body-centered tetragonal structured calcium molybdate with narrow nanosized distribution was detected using XRD, SAED and TEM. A diffraction pattern was also simulated and was found to be in accordance with those obtained from the experiment and JCPDS standard. Raman and FTIR spectra show the Mo-O prominent stretching bands in the [MoO 4] 2- tetrahedrons at 879.59 and 743-895 cm -1, respectively. Photoluminescence emission of CaMoO 4 was detected at 477 nm, caused by the annihilation of a self-trapped excitons from the [MoO 4] 2- excited complex. © 2009 Elsevier B.V. All rights reserved. |
format |
Journal |
author |
Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem |
author_facet |
Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem |
author_sort |
Anukorn Phuruangrat |
title |
Preparation, characterization and photoluminescence of nanocrystalline calcium molybdate |
title_short |
Preparation, characterization and photoluminescence of nanocrystalline calcium molybdate |
title_full |
Preparation, characterization and photoluminescence of nanocrystalline calcium molybdate |
title_fullStr |
Preparation, characterization and photoluminescence of nanocrystalline calcium molybdate |
title_full_unstemmed |
Preparation, characterization and photoluminescence of nanocrystalline calcium molybdate |
title_sort |
preparation, characterization and photoluminescence of nanocrystalline calcium molybdate |
publishDate |
2018 |
url |
https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=67649270499&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/49082 |
_version_ |
1681423346023006208 |