Effects of ethylenediamine to water ratios on cadmium sulfide nanorods and nanoparticles produced by a solvothermal method
Cadmium sulfide nanorods and nanoparticles were successfully produced by a solvothermal reaction at 200 °C for 24 h using ethylenediamine and water as pure and mixed solvents. The products were analyzed by X-ray diffraction, Raman spectroscopy and transmission electron microscopy. In pure ethylenedi...
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| Main Authors: | , , |
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| Format: | Journal |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=65549090016&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/49083 |
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| Institution: | Chiang Mai University |
| Summary: | Cadmium sulfide nanorods and nanoparticles were successfully produced by a solvothermal reaction at 200 °C for 24 h using ethylenediamine and water as pure and mixed solvents. The products were analyzed by X-ray diffraction, Raman spectroscopy and transmission electron microscopy. In pure ethylenediamine, they show the hexagonal structure CdS nanorods with 0.2-2 μm long and 30 nm diameter, and the 1LO and 2LO modes at 299.36 and 600.72 cm- 1, respectively. Growth of CdS nanorods is along the [001] direction, interpreted by HRTEM images and SAED patterns. In the 50:50 vol.% of ethylenediamine:water mixed solvents, the length of CdS nanorods decreased to 100-200 nm. The CdS nanoparticles were produced when pure water was used. © 2009 Elsevier B.V. All rights reserved. |
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