Characterization of copper sulfide hexananoplates, and nanoparticles synthesized by a sonochemical method
CuS hexanoplates and nanoparticles were prepared by sonochemical method in ethylene glycol as a solvent for 5 h. The products were characterized by X-ray diffraction (XRD), Raman spectroscopy, transmission electron microscopy (TEM), and energy dispersive X-ray (EDX) analysis. X-ray diffraction patte...
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| Main Authors: | , , |
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| Format: | Journal |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=79957903423&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/49840 |
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| Institution: | Chiang Mai University |
| Summary: | CuS hexanoplates and nanoparticles were prepared by sonochemical method in ethylene glycol as a solvent for 5 h. The products were characterized by X-ray diffraction (XRD), Raman spectroscopy, transmission electron microscopy (TEM), and energy dispersive X-ray (EDX) analysis. X-ray diffraction patterns detected only pure hexagonal CuS phase. Raman spectra show peaks at 473 cm-1, corresponding to the lattice vibration mode of S-S. Their morphologies were investigated by transmission electron microcopy, and the stoichiometric formula was also quantified. |
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