Cyclic microwave-assisted synthesis of Cu<inf>3</inf>BiS<inf>3</inf>dendrites using L-cysteine as a sulfur source and complexing agent
Nanostructured Cu3BiS3dendrites were successfully synthesized from CuCl, BiCl3and L-cysteine in ethylene glycol (EG), using cyclic microwave radiation (CMR). The phase was detected by X-ray diffraction (XRD) and selected area electron diffraction (SAED), and was in accordance with that obtained by t...
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| التنسيق: | دورية |
| منشور في: |
2018
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| الوصول للمادة أونلاين: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=78649323463&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/49986 |
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th-cmuir.6653943832-499862018-09-04T04:30:35Z Cyclic microwave-assisted synthesis of Cu<inf>3</inf>BiS<inf>3</inf>dendrites using L-cysteine as a sulfur source and complexing agent Kamonwan Aup-Ngoen Somchai Thongtem Titipun Thongtem Engineering Materials Science Physics and Astronomy Nanostructured Cu3BiS3dendrites were successfully synthesized from CuCl, BiCl3and L-cysteine in ethylene glycol (EG), using cyclic microwave radiation (CMR). The phase was detected by X-ray diffraction (XRD) and selected area electron diffraction (SAED), and was in accordance with that obtained by the simulation. Scanning and transmission electron microscopic (SEM and TEM) techniques revealed the gradual transformation of nanoparticles to nanostructured dendrites, due to the increase of microwave power. Photoluminescence of Cu3BiS3dendrites was a blue emission centered at 367 nm. © 2010 Elsevier B.V. All rights reserved. 2018-09-04T04:21:18Z 2018-09-04T04:21:18Z 2011-02-15 Journal 0167577X 2-s2.0-78649323463 10.1016/j.matlet.2010.10.047 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=78649323463&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/49986 |
| institution |
Chiang Mai University |
| building |
Chiang Mai University Library |
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Thailand |
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CMU Intellectual Repository |
| topic |
Engineering Materials Science Physics and Astronomy |
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Engineering Materials Science Physics and Astronomy Kamonwan Aup-Ngoen Somchai Thongtem Titipun Thongtem Cyclic microwave-assisted synthesis of Cu<inf>3</inf>BiS<inf>3</inf>dendrites using L-cysteine as a sulfur source and complexing agent |
| description |
Nanostructured Cu3BiS3dendrites were successfully synthesized from CuCl, BiCl3and L-cysteine in ethylene glycol (EG), using cyclic microwave radiation (CMR). The phase was detected by X-ray diffraction (XRD) and selected area electron diffraction (SAED), and was in accordance with that obtained by the simulation. Scanning and transmission electron microscopic (SEM and TEM) techniques revealed the gradual transformation of nanoparticles to nanostructured dendrites, due to the increase of microwave power. Photoluminescence of Cu3BiS3dendrites was a blue emission centered at 367 nm. © 2010 Elsevier B.V. All rights reserved. |
| format |
Journal |
| author |
Kamonwan Aup-Ngoen Somchai Thongtem Titipun Thongtem |
| author_facet |
Kamonwan Aup-Ngoen Somchai Thongtem Titipun Thongtem |
| author_sort |
Kamonwan Aup-Ngoen |
| title |
Cyclic microwave-assisted synthesis of Cu<inf>3</inf>BiS<inf>3</inf>dendrites using L-cysteine as a sulfur source and complexing agent |
| title_short |
Cyclic microwave-assisted synthesis of Cu<inf>3</inf>BiS<inf>3</inf>dendrites using L-cysteine as a sulfur source and complexing agent |
| title_full |
Cyclic microwave-assisted synthesis of Cu<inf>3</inf>BiS<inf>3</inf>dendrites using L-cysteine as a sulfur source and complexing agent |
| title_fullStr |
Cyclic microwave-assisted synthesis of Cu<inf>3</inf>BiS<inf>3</inf>dendrites using L-cysteine as a sulfur source and complexing agent |
| title_full_unstemmed |
Cyclic microwave-assisted synthesis of Cu<inf>3</inf>BiS<inf>3</inf>dendrites using L-cysteine as a sulfur source and complexing agent |
| title_sort |
cyclic microwave-assisted synthesis of cu<inf>3</inf>bis<inf>3</inf>dendrites using l-cysteine as a sulfur source and complexing agent |
| publishDate |
2018 |
| url |
https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=78649323463&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/49986 |
| _version_ |
1681423508661338112 |