Microwave-assisted synthesis and characterization of roselike and flower-like zinc oxide nanostructures
Hexagonal zinc oxide was synthesized by 180 W, 20 min microwave heating of 1:5 and 1:12.5 mole ratios of zinc chloride and sodium hydroxide as starting materials in aqueous solution system. The products were characterized using X-ray diffraction (XRD), scanning and transmission electron microscopy (...
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| Main Authors: | , , , |
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| Format: | Journal |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84864097736&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50061 |
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| Institution: | Chiang Mai University |
| Summary: | Hexagonal zinc oxide was synthesized by 180 W, 20 min microwave heating of 1:5 and 1:12.5 mole ratios of zinc chloride and sodium hydroxide as starting materials in aqueous solution system. The products were characterized using X-ray diffraction (XRD), scanning and transmission electron microscopy (SEM, TEM), and Fourier transform infrared (FTIR) and Raman spectroscopy. Rose-like particles of nanoplates and flower-like particles of nanorods of hexagonal zinc oxide with optical phonon E 2 vibration mode at 440 cm -1, and the stretching modes of Zn-O at 426 and 565 cm -1 were detected. |
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