Preparation of CCTO powders and ceramics by a simple solid state mixed oxide method

In this research, CaCu3.1Ti4O12.1: CC(3.1)TO ceramics were prepared by a simple solid state mixed oxide method. The optimum temperature for calcination the formation of phase pure perovskite and lattice parameters "a" of unit cell close to lattice parameter in the basis JCPDS file was foun...

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Main Authors: Chompoonuch Puchmark, Gobwute Rujijanagul
Format: Journal
Published: 2018
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Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=79960739936&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50076
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-500762018-09-04T04:30:02Z Preparation of CCTO powders and ceramics by a simple solid state mixed oxide method Chompoonuch Puchmark Gobwute Rujijanagul Materials Science Physics and Astronomy In this research, CaCu3.1Ti4O12.1: CC(3.1)TO ceramics were prepared by a simple solid state mixed oxide method. The optimum temperature for calcination the formation of phase pure perovskite and lattice parameters "a" of unit cell close to lattice parameter in the basis JCPDS file was found about 900°C for 8 h. Phase formation was examined by X-ray diffraction technique. The sintering process was carried out at 1000, 1025 and 1050°C for 8 h. The results show that the microstructure of fracture mode for variation sintered samples change from intergranular to intragranular mode with increasing sintering temperature. The density, average grain size, Vickers hardness and dielectric constant were increased with increasing the sintering temperature. Copyright © Taylor &Francis Group, LLC. 2018-09-04T04:23:26Z 2018-09-04T04:23:26Z 2011-07-29 Journal 15635112 00150193 2-s2.0-79960739936 10.1080/00150193.2011.577380 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=79960739936&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50076
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Materials Science
Physics and Astronomy
spellingShingle Materials Science
Physics and Astronomy
Chompoonuch Puchmark
Gobwute Rujijanagul
Preparation of CCTO powders and ceramics by a simple solid state mixed oxide method
description In this research, CaCu3.1Ti4O12.1: CC(3.1)TO ceramics were prepared by a simple solid state mixed oxide method. The optimum temperature for calcination the formation of phase pure perovskite and lattice parameters "a" of unit cell close to lattice parameter in the basis JCPDS file was found about 900°C for 8 h. Phase formation was examined by X-ray diffraction technique. The sintering process was carried out at 1000, 1025 and 1050°C for 8 h. The results show that the microstructure of fracture mode for variation sintered samples change from intergranular to intragranular mode with increasing sintering temperature. The density, average grain size, Vickers hardness and dielectric constant were increased with increasing the sintering temperature. Copyright © Taylor &Francis Group, LLC.
format Journal
author Chompoonuch Puchmark
Gobwute Rujijanagul
author_facet Chompoonuch Puchmark
Gobwute Rujijanagul
author_sort Chompoonuch Puchmark
title Preparation of CCTO powders and ceramics by a simple solid state mixed oxide method
title_short Preparation of CCTO powders and ceramics by a simple solid state mixed oxide method
title_full Preparation of CCTO powders and ceramics by a simple solid state mixed oxide method
title_fullStr Preparation of CCTO powders and ceramics by a simple solid state mixed oxide method
title_full_unstemmed Preparation of CCTO powders and ceramics by a simple solid state mixed oxide method
title_sort preparation of ccto powders and ceramics by a simple solid state mixed oxide method
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=79960739936&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50076
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