Microwave-assisted hydrothermal synthesis of lead zirconate fine powders

Microwave-assisted hydrothermal synthesis of lead zirconate fine powders

A rapid synthesis of lead zirconate fine powders by microwave-assisted hydrothermal technique is reported. The influences of type of lead precursor, concentration of potassium hydroxide mineraliser, applied microwave power and irradiation time are described. The synthesised powders were characterise...

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Main Authors: Saowalak Tapala, Apinpus Rujiwatra
Format: Journal
Published: 2018
Subjects:
Multidisciplinary
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=79953037842&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50388
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-503882018-09-04T04:31:45Z Microwave-assisted hydrothermal synthesis of lead zirconate fine powders Saowalak Tapala Apinpus Rujiwatra Multidisciplinary A rapid synthesis of lead zirconate fine powders by microwave-assisted hydrothermal technique is reported. The influences of type of lead precursor, concentration of potassium hydroxide mineraliser, applied microwave power and irradiation time are described. The synthesised powders were characterised by powder X-ray diffraction, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopic microanalysis and light scattering technique. The merits of the microwave application in reducing reaction time and improving particle mono-dispersion and size uniformity as well as the drawbacks, viz. low purity of the desired phase and increasing demand of mineraliser, are discussed in relation to conventional heating method. © 2011 by Maejo University, San Sai, Chiang Mai, 50290 Thailand. 2018-09-04T04:31:45Z 2018-09-04T04:31:45Z 2011-01-01 Journal 19057873 2-s2.0-79953037842 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=79953037842&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50388
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Multidisciplinary
spellingShingle Multidisciplinary
Saowalak Tapala
Apinpus Rujiwatra
Microwave-assisted hydrothermal synthesis of lead zirconate fine powders
description A rapid synthesis of lead zirconate fine powders by microwave-assisted hydrothermal technique is reported. The influences of type of lead precursor, concentration of potassium hydroxide mineraliser, applied microwave power and irradiation time are described. The synthesised powders were characterised by powder X-ray diffraction, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopic microanalysis and light scattering technique. The merits of the microwave application in reducing reaction time and improving particle mono-dispersion and size uniformity as well as the drawbacks, viz. low purity of the desired phase and increasing demand of mineraliser, are discussed in relation to conventional heating method. © 2011 by Maejo University, San Sai, Chiang Mai, 50290 Thailand.
format Journal
author Saowalak Tapala
Apinpus Rujiwatra
author_facet Saowalak Tapala
Apinpus Rujiwatra
author_sort Saowalak Tapala
title Microwave-assisted hydrothermal synthesis of lead zirconate fine powders
title_short Microwave-assisted hydrothermal synthesis of lead zirconate fine powders
title_full Microwave-assisted hydrothermal synthesis of lead zirconate fine powders
title_fullStr Microwave-assisted hydrothermal synthesis of lead zirconate fine powders
title_full_unstemmed Microwave-assisted hydrothermal synthesis of lead zirconate fine powders
title_sort microwave-assisted hydrothermal synthesis of lead zirconate fine powders
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=79953037842&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50388
_version_ 1681423580901933056

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