Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes
CdS (hcp) crystals were synthesized using CdCl2.2H2O in C4H11N containing 20% (NH4)2S by the 5 h sonochemical process followed by the hydrothermal reaction at different temperatures and times. CdS (hcp) crystals composing of Cd and S were detected using XRD, SAED and EDX. A Raman spectrometer reveal...
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th-cmuir.6653943832-506632018-09-04T04:53:18Z Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Chemistry Materials Science Physics and Astronomy CdS (hcp) crystals were synthesized using CdCl2.2H2O in C4H11N containing 20% (NH4)2S by the 5 h sonochemical process followed by the hydrothermal reaction at different temperatures and times. CdS (hcp) crystals composing of Cd and S were detected using XRD, SAED and EDX. A Raman spectrometer revealed the presence of fundamental and overtone modes at 299 and 596 cm-1, respectively. The crystals are nanorods growing in systematic array analyzed using TEM and HRTEM. Their photoluminescence is in the blue spectral region at 409-422 nm (2.94-3.03 eV). 2018-09-04T04:43:35Z 2018-09-04T04:43:35Z 2010-09-01 Journal 15848663 2-s2.0-78249246321 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=78249246321&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50663 |
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Chemistry Materials Science Physics and Astronomy Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes |
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CdS (hcp) crystals were synthesized using CdCl2.2H2O in C4H11N containing 20% (NH4)2S by the 5 h sonochemical process followed by the hydrothermal reaction at different temperatures and times. CdS (hcp) crystals composing of Cd and S were detected using XRD, SAED and EDX. A Raman spectrometer revealed the presence of fundamental and overtone modes at 299 and 596 cm-1, respectively. The crystals are nanorods growing in systematic array analyzed using TEM and HRTEM. Their photoluminescence is in the blue spectral region at 409-422 nm (2.94-3.03 eV). |
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Journal |
author |
Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem |
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Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem |
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Anukorn Phuruangrat |
title |
Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes |
title_short |
Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes |
title_full |
Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes |
title_fullStr |
Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes |
title_full_unstemmed |
Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes |
title_sort |
two-step synthesis of cds (hcp) nanorods using sonochemical and hydrothermal processes |
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2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=78249246321&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50663 |
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