Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes

CdS (hcp) crystals were synthesized using CdCl2.2H2O in C4H11N containing 20% (NH4)2S by the 5 h sonochemical process followed by the hydrothermal reaction at different temperatures and times. CdS (hcp) crystals composing of Cd and S were detected using XRD, SAED and EDX. A Raman spectrometer reveal...

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Main Authors: Anukorn Phuruangrat, Titipun Thongtem, Somchai Thongtem
Format: Journal
Published: 2018
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http://cmuir.cmu.ac.th/jspui/handle/6653943832/50663
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-506632018-09-04T04:53:18Z Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Chemistry Materials Science Physics and Astronomy CdS (hcp) crystals were synthesized using CdCl2.2H2O in C4H11N containing 20% (NH4)2S by the 5 h sonochemical process followed by the hydrothermal reaction at different temperatures and times. CdS (hcp) crystals composing of Cd and S were detected using XRD, SAED and EDX. A Raman spectrometer revealed the presence of fundamental and overtone modes at 299 and 596 cm-1, respectively. The crystals are nanorods growing in systematic array analyzed using TEM and HRTEM. Their photoluminescence is in the blue spectral region at 409-422 nm (2.94-3.03 eV). 2018-09-04T04:43:35Z 2018-09-04T04:43:35Z 2010-09-01 Journal 15848663 2-s2.0-78249246321 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=78249246321&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50663
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Chemistry
Materials Science
Physics and Astronomy
spellingShingle Chemistry
Materials Science
Physics and Astronomy
Anukorn Phuruangrat
Titipun Thongtem
Somchai Thongtem
Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes
description CdS (hcp) crystals were synthesized using CdCl2.2H2O in C4H11N containing 20% (NH4)2S by the 5 h sonochemical process followed by the hydrothermal reaction at different temperatures and times. CdS (hcp) crystals composing of Cd and S were detected using XRD, SAED and EDX. A Raman spectrometer revealed the presence of fundamental and overtone modes at 299 and 596 cm-1, respectively. The crystals are nanorods growing in systematic array analyzed using TEM and HRTEM. Their photoluminescence is in the blue spectral region at 409-422 nm (2.94-3.03 eV).
format Journal
author Anukorn Phuruangrat
Titipun Thongtem
Somchai Thongtem
author_facet Anukorn Phuruangrat
Titipun Thongtem
Somchai Thongtem
author_sort Anukorn Phuruangrat
title Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes
title_short Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes
title_full Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes
title_fullStr Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes
title_full_unstemmed Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes
title_sort two-step synthesis of cds (hcp) nanorods using sonochemical and hydrothermal processes
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=78249246321&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50663
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