One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate
Phase-pure and stoichiometric lead zirconate powders consisting of submicro- to micrometer-sized particles were successfully synthesized via a simple, one-pot hydrothermal technique at moderate temperatures and short reaction times. High concentration of potassium hydroxide mineralizer was necessary...
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2014
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th-cmuir.6653943832-50732014-08-30T02:56:07Z One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate Rujiwatra A. Tapala S. Luachan S. Khamman O. Ananta S. Phase-pure and stoichiometric lead zirconate powders consisting of submicro- to micrometer-sized particles were successfully synthesized via a simple, one-pot hydrothermal technique at moderate temperatures and short reaction times. High concentration of potassium hydroxide mineralizer was necessary in the formation of well-crystalline lead zirconate. The type of zirconium precursor, reaction temperature and time showed apparent influences over particle shape, size and distribution. Transmission electron microscope was used to confirm the crystallographic setting of the prepared lead zirconate. © 2006 Elsevier B.V. All rights reserved. 2014-08-30T02:56:07Z 2014-08-30T02:56:07Z 2006 Article 0167577X 10.1016/j.matlet.2006.02.010 MLETD http://www.scopus.com/inward/record.url?eid=2-s2.0-33746368694&partnerID=40&md5=05109e2d6585e730001765a6c9d6797e http://cmuir.cmu.ac.th/handle/6653943832/5073 English |
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| description |
Phase-pure and stoichiometric lead zirconate powders consisting of submicro- to micrometer-sized particles were successfully synthesized via a simple, one-pot hydrothermal technique at moderate temperatures and short reaction times. High concentration of potassium hydroxide mineralizer was necessary in the formation of well-crystalline lead zirconate. The type of zirconium precursor, reaction temperature and time showed apparent influences over particle shape, size and distribution. Transmission electron microscope was used to confirm the crystallographic setting of the prepared lead zirconate. © 2006 Elsevier B.V. All rights reserved. |
| format |
Article |
| author |
Rujiwatra A. Tapala S. Luachan S. Khamman O. Ananta S. |
| spellingShingle |
Rujiwatra A. Tapala S. Luachan S. Khamman O. Ananta S. One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate |
| author_facet |
Rujiwatra A. Tapala S. Luachan S. Khamman O. Ananta S. |
| author_sort |
Rujiwatra A. |
| title |
One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate |
| title_short |
One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate |
| title_full |
One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate |
| title_fullStr |
One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate |
| title_full_unstemmed |
One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate |
| title_sort |
one-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-33746368694&partnerID=40&md5=05109e2d6585e730001765a6c9d6797e http://cmuir.cmu.ac.th/handle/6653943832/5073 |
| _version_ |
1681420356554850304 |