Cyclic microwave assisted synthesis of Sb2S3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent

Cyclic microwave assisted synthesis of Sb2S3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent

Antimony sulfide (Sb2S3) was successfully synthesized from antimony chloride (SbCl3) and sodiumthiosulfate (Na2S2O3) in ethylene glycol (EG) containing different polyvinylpyrrolidone (PVP) masses under cyclic microwave radiation. XRD and SEM show that the products were orthorhombic Sb2S3nanorods for...

Full description

Saved in:
Bibliographic Details
Main Authors: Jutarat Kavinchan, Titipun Thongtem, Somchai Thongtem
Format: Journal
Published: 2018
Subjects:
Engineering
Materials Science
Physics and Astronomy
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77955704851&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50794
Tags: Add Tag
No Tags, Be the first to tag this record!
Institution: Chiang Mai University
id th-cmuir.6653943832-50794
record_format dspace
spelling th-cmuir.6653943832-507942018-09-04T04:53:11Z Cyclic microwave assisted synthesis of Sb2S3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent Jutarat Kavinchan Titipun Thongtem Somchai Thongtem Engineering Materials Science Physics and Astronomy Antimony sulfide (Sb2S3) was successfully synthesized from antimony chloride (SbCl3) and sodiumthiosulfate (Na2S2O3) in ethylene glycol (EG) containing different polyvinylpyrrolidone (PVP) masses under cyclic microwave radiation. XRD and SEM show that the products were orthorhombic Sb2S3nanorods forming the dumb-bells. TEM study reveals Sb2S3single-crystal nanorods, growing along the [001] direction. The dumb-bell formation is also proposed, according to the splitting ends and a middle tie-up. Its direct band gap, calculated from UV-visible absorption, is 1.52 eV. © 2010 Elsevier B.V. 2018-09-04T04:45:40Z 2018-09-04T04:45:40Z 2010-11-15 Journal 0167577X 2-s2.0-77955704851 10.1016/j.matlet.2010.07.075 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77955704851&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50794
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Engineering
Materials Science
Physics and Astronomy
spellingShingle Engineering
Materials Science
Physics and Astronomy
Jutarat Kavinchan
Titipun Thongtem
Somchai Thongtem
Cyclic microwave assisted synthesis of Sb2S3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent
description Antimony sulfide (Sb2S3) was successfully synthesized from antimony chloride (SbCl3) and sodiumthiosulfate (Na2S2O3) in ethylene glycol (EG) containing different polyvinylpyrrolidone (PVP) masses under cyclic microwave radiation. XRD and SEM show that the products were orthorhombic Sb2S3nanorods forming the dumb-bells. TEM study reveals Sb2S3single-crystal nanorods, growing along the [001] direction. The dumb-bell formation is also proposed, according to the splitting ends and a middle tie-up. Its direct band gap, calculated from UV-visible absorption, is 1.52 eV. © 2010 Elsevier B.V.
format Journal
author Jutarat Kavinchan
Titipun Thongtem
Somchai Thongtem
author_facet Jutarat Kavinchan
Titipun Thongtem
Somchai Thongtem
author_sort Jutarat Kavinchan
title Cyclic microwave assisted synthesis of Sb2S3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent
title_short Cyclic microwave assisted synthesis of Sb2S3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent
title_full Cyclic microwave assisted synthesis of Sb2S3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent
title_fullStr Cyclic microwave assisted synthesis of Sb2S3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent
title_full_unstemmed Cyclic microwave assisted synthesis of Sb2S3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent
title_sort cyclic microwave assisted synthesis of sb2s3 dumb-bells using polyvinylpyrrolidone as a template and splitting agent
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77955704851&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50794
_version_ 1681423653983485952

Similar Items