Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent

Double-sheaves of antimony sulfide were synthesized by the 200 °C and 24 h hydrothermal reaction in the acidic solution, containing copolymer - a crystal splitting agent. Using X-ray technique, electron microscopy, and Raman as well as UV-visible NIR absorption spectroscopy, the products were specif...

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Main Authors:	Chalermchai Pilapong, Titipun Thongtem, Somchai Thongtem
Format:	Journal
Published:	2018
Subjects:	Engineering Materials Science
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77957103934&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50796
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Institution:	Chiang Mai University

id	th-cmuir.6653943832-50796
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spelling	th-cmuir.6653943832-507962018-09-04T04:48:06Z Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent Chalermchai Pilapong Titipun Thongtem Somchai Thongtem Engineering Materials Science Double-sheaves of antimony sulfide were synthesized by the 200 °C and 24 h hydrothermal reaction in the acidic solution, containing copolymer - a crystal splitting agent. Using X-ray technique, electron microscopy, and Raman as well as UV-visible NIR absorption spectroscopy, the products were specified as orthorhombic Sb2S3, composing of Sb and S with five vibration modes, in the shape of spears in bundles with the [0 0 1] growth direction and 2.38 eV direct energy gap. A diffraction pattern was also simulated, and is in good accordance with that obtained by the interpretation. © 2010 Elsevier B.V. All rights reserved. 2018-09-04T04:45:45Z 2018-09-04T04:45:45Z 2010-10-08 Journal 09258388 2-s2.0-77957103934 10.1016/j.jallcom.2010.08.003 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77957103934&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50796
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Engineering Materials Science
spellingShingle	Engineering Materials Science Chalermchai Pilapong Titipun Thongtem Somchai Thongtem Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent
description	Double-sheaves of antimony sulfide were synthesized by the 200 °C and 24 h hydrothermal reaction in the acidic solution, containing copolymer - a crystal splitting agent. Using X-ray technique, electron microscopy, and Raman as well as UV-visible NIR absorption spectroscopy, the products were specified as orthorhombic Sb2S3, composing of Sb and S with five vibration modes, in the shape of spears in bundles with the [0 0 1] growth direction and 2.38 eV direct energy gap. A diffraction pattern was also simulated, and is in good accordance with that obtained by the interpretation. © 2010 Elsevier B.V. All rights reserved.
format	Journal
author	Chalermchai Pilapong Titipun Thongtem Somchai Thongtem
author_facet	Chalermchai Pilapong Titipun Thongtem Somchai Thongtem
author_sort	Chalermchai Pilapong
title	Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent
title_short	Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent
title_full	Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent
title_fullStr	Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent
title_full_unstemmed	Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent
title_sort	hydrothermal synthesis of double sheaf-like sb2s3 using copolymer as a crystal splitting agent
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77957103934&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50796
_version_	1681423654331613184

Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent

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