Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation

Nanocrystalline compounds MMoO4 (M = Ca, Sr and Ba) were synthesized in propylene glycol using cyclic microwave radiation. XRD, TEM, SAED and EDX analyses revealed the presence of nanocrystallites of the phases containing the corresponding alkaline earth metals, Mo and O. The calculated lattice para...

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Main Authors:	A. Phuruangrat, T. Thongtem, S. Thongtem
Format:	Journal
Published:	2018
Subjects:	Engineering Materials Science Physics and Astronomy
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77956622992&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50799
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Institution:	Chiang Mai University

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spelling	th-cmuir.6653943832-507992018-09-04T04:53:15Z Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation A. Phuruangrat T. Thongtem S. Thongtem Engineering Materials Science Physics and Astronomy Nanocrystalline compounds MMoO4 (M = Ca, Sr and Ba) were synthesized in propylene glycol using cyclic microwave radiation. XRD, TEM, SAED and EDX analyses revealed the presence of nanocrystallites of the phases containing the corresponding alkaline earth metals, Mo and O. The calculated lattice parameters and the crystallite sizes both increased with the increase in the atomic masses and the ionic radii of the divalent metals. Six different vibrations were detected using Raman spectroscopy, and very strong Mo-O stretching mode of [MoO4]2- tetrahedrons was observed using FTIR. 2018-09-04T04:45:46Z 2018-09-04T04:45:46Z 2010-09-21 Journal 01371339 2-s2.0-77956622992 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77956622992&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50799
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Engineering Materials Science Physics and Astronomy
spellingShingle	Engineering Materials Science Physics and Astronomy A. Phuruangrat T. Thongtem S. Thongtem Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation
description	Nanocrystalline compounds MMoO4 (M = Ca, Sr and Ba) were synthesized in propylene glycol using cyclic microwave radiation. XRD, TEM, SAED and EDX analyses revealed the presence of nanocrystallites of the phases containing the corresponding alkaline earth metals, Mo and O. The calculated lattice parameters and the crystallite sizes both increased with the increase in the atomic masses and the ionic radii of the divalent metals. Six different vibrations were detected using Raman spectroscopy, and very strong Mo-O stretching mode of [MoO4]2- tetrahedrons was observed using FTIR.
format	Journal
author	A. Phuruangrat T. Thongtem S. Thongtem
author_facet	A. Phuruangrat T. Thongtem S. Thongtem
author_sort	A. Phuruangrat
title	Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation
title_short	Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation
title_full	Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation
title_fullStr	Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation
title_full_unstemmed	Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation
title_sort	synthesis of nanocrystalline metal molybdates using cyclic microwave radiation
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77956622992&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50799
_version_	1681423654856949760

Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation

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