Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles

Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles

Bi2S3nanorods in flower-shaped bundles were successfully synthesized from the decomposition of Bithiourea complexes under the microwave-assisted hydrothermal process. X-ray powder diffraction (XRD) patterns and field emission scanning electron microscopy (FE-SEM) show that Bi2S3has the orthorhombic...

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Main Authors: Titipun Thongtem, Chalermchai Pilapong, Jutarat Kavinchan, Anukorn Phuruangrat, Somchai Thongtem
Format: Journal
Published: 2018
Subjects:
Engineering
Materials Science
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77954217737&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50809
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-508092018-09-04T04:48:20Z Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles Titipun Thongtem Chalermchai Pilapong Jutarat Kavinchan Anukorn Phuruangrat Somchai Thongtem Engineering Materials Science Bi2S3nanorods in flower-shaped bundles were successfully synthesized from the decomposition of Bithiourea complexes under the microwave-assisted hydrothermal process. X-ray powder diffraction (XRD) patterns and field emission scanning electron microscopy (FE-SEM) show that Bi2S3has the orthorhombic phase and appears as nanorods in flower-shaped bundles. A transmission electron microscopic (TEM) study reveals the independent single Bi2S3nanorods with their growth along the [0 0 1] direction. A possible formation mechanism of Bi2S3nanorods in flower-shaped bundles is also proposed and discussed. Their UVvis spectrum shows the absorbance at 596 nm, with its direct energy band gap of 1.82 eV. © 2009 Elsevier B.V. 2018-09-04T04:46:02Z 2018-09-04T04:46:02Z 2010-06-25 Journal 09258388 2-s2.0-77954217737 10.1016/j.jallcom.2010.03.240 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77954217737&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50809
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Engineering
Materials Science
spellingShingle Engineering
Materials Science
Titipun Thongtem
Chalermchai Pilapong
Jutarat Kavinchan
Anukorn Phuruangrat
Somchai Thongtem
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles
description Bi2S3nanorods in flower-shaped bundles were successfully synthesized from the decomposition of Bithiourea complexes under the microwave-assisted hydrothermal process. X-ray powder diffraction (XRD) patterns and field emission scanning electron microscopy (FE-SEM) show that Bi2S3has the orthorhombic phase and appears as nanorods in flower-shaped bundles. A transmission electron microscopic (TEM) study reveals the independent single Bi2S3nanorods with their growth along the [0 0 1] direction. A possible formation mechanism of Bi2S3nanorods in flower-shaped bundles is also proposed and discussed. Their UVvis spectrum shows the absorbance at 596 nm, with its direct energy band gap of 1.82 eV. © 2009 Elsevier B.V.
format Journal
author Titipun Thongtem
Chalermchai Pilapong
Jutarat Kavinchan
Anukorn Phuruangrat
Somchai Thongtem
author_facet Titipun Thongtem
Chalermchai Pilapong
Jutarat Kavinchan
Anukorn Phuruangrat
Somchai Thongtem
author_sort Titipun Thongtem
title Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles
title_short Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles
title_full Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles
title_fullStr Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles
title_full_unstemmed Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles
title_sort microwave-assisted hydrothermal synthesis of bi2s3 nanorods in flower-shaped bundles
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77954217737&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50809
_version_ 1681423656664694784

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