Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction

AgBiS2nanostructured flowers were produced from CH3COOAg, Bi(NO3)3.5H2O and thiosemicarbazide (NH2CSNHNH2) using different solvents [ethylene glycol (EG), water (H2O), polyethylene glycol with molecular weight of 200 (PEG200), and propylene glycol (PG)] in Teflon-lined stainless steel autoclaves. Th...

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Main Authors: Titipun Thongtem, Narongrit Tipcompor, Somchai Thongtem
Format: Journal
Published: 2018
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http://cmuir.cmu.ac.th/jspui/handle/6653943832/50835
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-508352018-09-04T04:53:39Z Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction Titipun Thongtem Narongrit Tipcompor Somchai Thongtem Engineering Materials Science Physics and Astronomy AgBiS2nanostructured flowers were produced from CH3COOAg, Bi(NO3)3.5H2O and thiosemicarbazide (NH2CSNHNH2) using different solvents [ethylene glycol (EG), water (H2O), polyethylene glycol with molecular weight of 200 (PEG200), and propylene glycol (PG)] in Teflon-lined stainless steel autoclaves. The phase and purity were detected using X-ray diffraction (XRD), controlled by the solvents. The product was purified AgBiS2produced by the 200 °C and 24 h reaction in EG, corresponding to selected area electron diffraction (SAED) and simulation patterns. Scanning and transmission electron microscopies (SEM and TEM) revealed the formation of nanostructured flowers - enlarged by the increase in the lengths of time and temperature. Their photoluminescence (PL) emissions were detected at the same wavelength of 382 nm (3.24 eV), although they were produced under different conditions. © 2010 Elsevier B.V. All rights reserved. 2018-09-04T04:46:21Z 2018-09-04T04:46:21Z 2010-03-31 Journal 0167577X 2-s2.0-75749097711 10.1016/j.matlet.2010.01.003 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75749097711&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50835
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Engineering
Materials Science
Physics and Astronomy
spellingShingle Engineering
Materials Science
Physics and Astronomy
Titipun Thongtem
Narongrit Tipcompor
Somchai Thongtem
Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction
description AgBiS2nanostructured flowers were produced from CH3COOAg, Bi(NO3)3.5H2O and thiosemicarbazide (NH2CSNHNH2) using different solvents [ethylene glycol (EG), water (H2O), polyethylene glycol with molecular weight of 200 (PEG200), and propylene glycol (PG)] in Teflon-lined stainless steel autoclaves. The phase and purity were detected using X-ray diffraction (XRD), controlled by the solvents. The product was purified AgBiS2produced by the 200 °C and 24 h reaction in EG, corresponding to selected area electron diffraction (SAED) and simulation patterns. Scanning and transmission electron microscopies (SEM and TEM) revealed the formation of nanostructured flowers - enlarged by the increase in the lengths of time and temperature. Their photoluminescence (PL) emissions were detected at the same wavelength of 382 nm (3.24 eV), although they were produced under different conditions. © 2010 Elsevier B.V. All rights reserved.
format Journal
author Titipun Thongtem
Narongrit Tipcompor
Somchai Thongtem
author_facet Titipun Thongtem
Narongrit Tipcompor
Somchai Thongtem
author_sort Titipun Thongtem
title Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction
title_short Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction
title_full Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction
title_fullStr Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction
title_full_unstemmed Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction
title_sort characterization of agbis2 nanostructured flowers produced by solvothermal reaction
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75749097711&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50835
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