Characterization of SrCO3 and BaCO3 nanoparticles synthesized by sonochemical method
SrCO3and BaCO3nanoparticles were synthesized using Sr(NO3)2or Ba(NO3)2and Na2CO3as starting materials in ethylene glycol by ultrasonic irradiation at 80 °C for 1-5 h. Their phases, vibration modes and morphologies were characterized using X-ray powder diffraction (XRD), Fourier transform infrared (F...
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| Main Authors: | , , , |
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| Format: | Journal |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=72649095067&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50837 |
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| Institution: | Chiang Mai University |
| Summary: | SrCO3and BaCO3nanoparticles were synthesized using Sr(NO3)2or Ba(NO3)2and Na2CO3as starting materials in ethylene glycol by ultrasonic irradiation at 80 °C for 1-5 h. Their phases, vibration modes and morphologies were characterized using X-ray powder diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, selected area electron diffraction (SAED) and transmission electron microscopy (TEM). These products were found to be orthorhombic SrCO3and BaCO3nanoparticles with 20-50 nm and 40-100 nm ranges, respectively. Asymmetric stretching, symmetric stretching, and out of plane and in plane bending vibrations of CO32-complexes were also detected. © 2009 Elsevier B.V. All rights reserved. |
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