Characterization of Bi2S3 with different morphologies synthesized using microwave radiation

Bi2S3with different morphologies (nanoparticles, nanorods and nanotubes) was synthesized using bismuth nitrate pentahydrate (Bi(NO3)3·5H2O) and two kinds of sulfur sources (CH3CSNH2and NH2CSNH2) in different solvents (water, ethylene glycol and propylene glycol) via a microwave radiation method at 1...

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Main Authors: Titipun Thongtem, Anukorn Phuruangrat, Surangkana Wannapop, Somchai Thongtem
Format: Journal
Published: 2018
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http://cmuir.cmu.ac.th/jspui/handle/6653943832/50878
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-508782018-09-04T04:53:44Z Characterization of Bi2S3 with different morphologies synthesized using microwave radiation Titipun Thongtem Anukorn Phuruangrat Surangkana Wannapop Somchai Thongtem Engineering Materials Science Physics and Astronomy Bi2S3with different morphologies (nanoparticles, nanorods and nanotubes) was synthesized using bismuth nitrate pentahydrate (Bi(NO3)3·5H2O) and two kinds of sulfur sources (CH3CSNH2and NH2CSNH2) in different solvents (water, ethylene glycol and propylene glycol) via a microwave radiation method at 180 W for 20 min. X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) indicated that all of the products are orthorhombic Bi2S3phase of nanoparticles, nanorods and nanotubes, influenced by the sulfur sources and solvents. Formation mechanisms of the products with different morphologies are also proposed. © 2009 Elsevier B.V. All rights reserved. 2018-09-04T04:46:47Z 2018-09-04T04:46:47Z 2010-01-31 Journal 0167577X 2-s2.0-70449534600 10.1016/j.matlet.2009.10.006 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=70449534600&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50878
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Engineering
Materials Science
Physics and Astronomy
spellingShingle Engineering
Materials Science
Physics and Astronomy
Titipun Thongtem
Anukorn Phuruangrat
Surangkana Wannapop
Somchai Thongtem
Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
description Bi2S3with different morphologies (nanoparticles, nanorods and nanotubes) was synthesized using bismuth nitrate pentahydrate (Bi(NO3)3·5H2O) and two kinds of sulfur sources (CH3CSNH2and NH2CSNH2) in different solvents (water, ethylene glycol and propylene glycol) via a microwave radiation method at 180 W for 20 min. X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) indicated that all of the products are orthorhombic Bi2S3phase of nanoparticles, nanorods and nanotubes, influenced by the sulfur sources and solvents. Formation mechanisms of the products with different morphologies are also proposed. © 2009 Elsevier B.V. All rights reserved.
format Journal
author Titipun Thongtem
Anukorn Phuruangrat
Surangkana Wannapop
Somchai Thongtem
author_facet Titipun Thongtem
Anukorn Phuruangrat
Surangkana Wannapop
Somchai Thongtem
author_sort Titipun Thongtem
title Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_short Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_full Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_fullStr Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_full_unstemmed Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_sort characterization of bi2s3 with different morphologies synthesized using microwave radiation
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=70449534600&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/50878
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